نتایج جستجو برای: thermal decomposition of oxalate precursormethod

تعداد نتایج: 21192671  

Magnesium hydroxide nanostructures as an effective flame retardant were synthesized by a facile and rapid microwave reaction. The effect of different surfactants such as cationic, anionic and polymeric on the morphology of magnesium hydroxide nanostructures was investigated. Nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform in...

2009
Ya-Guang Sun Mei-yan Guo Gang Xiong Bing Jiang Lei Wang

Single crystals of KTb(C(2)O(4))(SO(4))(H(2)O), potassium aqua-terbium(III) oxalate sulfate, were obtained under hydro-thermal conditions. In the crystal structure, the Tb(III) atom is coordinated by four O atoms from two oxalate anions, three O atoms from three sulfate anions and one O atom from a water mol-ecule within a TbO(8) distorted square antiprismatic coordination. The potassium and te...

ژورنال: مواد پرانرژی 2016

In this research, the effects of the particle size and shape of aluminum powder on the kinetics and thermodynamic properties of HMX thermal decomposition in a PBX formulation were investigated. Nano-structured aluminum powder has flaked shape and thickness of about 20-30 nm. Kinetics and thermodynamic parameters were calculated by both Kissinger and Flynn-Wall-Ozawa (FWO) methods based on diffe...

Journal: :علوم و تکنولوژی پلیمر 0
مهدی باریکانی فهیمه عسکری مجید باریکانی محمد برمر

polyurethane foams are extensively used in different applications such as furnitures and sandwich structures due to better mechanical properties, higher acoustic and damping behavior, higher resistance to hydrocarbon, and aging.with respect to flammability of polyurethane materials and safety precaution in living and working environments there is a vital need to study and investigate published ...

ژورنال: مواد پرانرژی 2013

Abstract In this study, the effect of additives such as ammonium oxalate (AO), mixture of ammonium oxalate and strontium carbonate (SC) on AP/HTPB based composite propellants was investigated by burning rate, DTA, density and autoignition temperature measurements. The results show that the burning rates of these propellants are decreased significantly. DTA and autoignition temperature experime...

Composite solid propellants were prepared with and without nano-alloys (Ti-Co, Ti-Ni, Ti-Zn), where nano-alloys used as catalyst. These nano-alloys are prepared by hydrazine reduction method. Catalytic properties of these nanomaterials were measured on Ammonium perchorate/hydroxyterminatedpolybutadiene propellant by thermogravimetery analysis and differential thermal analysis. Both experimental...

2008
Zhen-Yu Xuan Yong Che Yong-Chun Huang

The title compound, [Ni(C(2)O(4))(C(5)H(5)N)(2)](n), was synthesized under hydro-(solvo)thermal conditions. The Ni(II) atom, lying on a twofold rotation axis, has an octa-hedral coordination geometry involving two N atoms from two pyridine ligands and four O atoms from two oxalate ligands. The Ni atoms are connected by the tetra-dentate bridging oxalate ligands into a one-dimensional zigzag chain.

ژورنال: مواد پرانرژی 2016
رضایی, منا, شهیدزاده, منصور,

polyester polyol can be used in high energy propellant as a binder.In this research, polyazido polyester was synthesized from direct polycondensation reaction between adipic acid and 2,2-bis(bromomethyl)-1,3-propanediol. Then, azidation of poly bromoester afford polyazidoester as an energetic polyester. polyazidoester have identified and characterized by FTIR,HNMR,GPC,DSC and elemental analysis...

2010
Anqiang Pan Ji-Guang Zhang Zimin Nie Guozhong Cao Bruce W. Arey Guosheng Li Shu-quan Liang Jun Liu

Nano-structured vanadium oxide (V2O5) is fabricated via a facile thermal-decomposition of vanadium precursor, vanadyl oxalate, which is produced by reacting micro-sized V2O5 with oxalic acid. The V2O5 nanoparticles produced by this method exhibit much better electrochemical performance than commercial micro-sized V2O5. The optimized-nanorod electrodes give the best specific discharge capacities...

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