The hydrodesulfurization (HDS) activity of molybdenum sulfide-based catalysts is localized to the edges of this layered solid and is, therefore, highly dependent on the technique used to prepare the material. Here, ultrasonic spray pyrolysis (USP) was used to synthesize porous, nanostructured MoS2. Low surface area powders, not useful for catalysis, are generally produced by USP. This work show...

Modern gas turbine hot sections need to be protected from elevated temperature and damaging environments. This protection starts as a typically two layer coating system, the base layer or bond coat (BC) acts as a corrosion barrier and a kind of buffer for the thermal mismatch between the base material and the second top thermally protective layer or Thermal Barrier Coating (TBC). The BC is norm...

Opadry® II 1 Influence of Film Coating Process Parameters on the Gloss of Tablets Coated with Pigmented Aqueous Film Coating Formulations PURPOSE A common practice for enhancing the gloss of coated tablets is the application of a clear top-coat after applying a pigmented coating layer. In a recent study, substantial increases in tablet gloss were achieved using this multiple step approach.1 It ...

Photoluminescence of highly structured ZnO layers comprising well-shaped hexagonal rods is presented. The ZnO rods (length 500-1,000 nm, diameter 100-300 nm) were grown in air onto a preheated soda-lime glass (SGL) or ITO/SGL substrate by low-cost chemical spray pyrolysis method using zinc chloride precursor solutions and growth temperatures in the range of 450-550°C. We report the effect of th...

the corrosion protection of mild steel by a newly developed epoxy-based coating system containing inherently conducting nanopolyaniline-clay as a nanoadditive has been studied. polyaniline-clay anticorrosion nanoadditive (pcna) was obtained by the direct mixing method of nanopolyaniline (0.03 wt.%) and organo-modified clay (3 wt.%) at atmospheric pressure, and xrd technique was used to study d-...

Porous carbon spheres with unique structures and morphologies are prepared from energetic carbon precursors, alkali propiolates, via ultrasonic spray pyrolysis. Aerosolized liquid droplets containing alkali propiolates act as microreactors that confine the thermal decomposition of energetic precursors and lead to the formation of several unprecedented carbon morphologies.

Carbon-iron oxide microspheres' black pigments (CIOMBs) had been prepared via ultrasonic spray pyrolysis of aqueous solutions containing ferrous chloride and glucose. Due to the presence of carbon, CIOMBs not only exhibited remarkably acid resistance, but also could be well dispersed in both polar solvents and nonpolar solvent. Finally, dispersions of hollow CIOMBs in tetrachloroethylene had su...

An indigenously developed chemical spray pyrolysis system was used to deposit polycrystalline CuInS2 thin films. It was found that smaller spray rate results in films with better crystallinity and lower resistivity. Increase in surface roughness of the films was observed for higher spray rates. Variations in film stoichiometry with composition of spray solution were analyzed along with its opto...

Pure and mixed ZnO-SiO2 particles were prepared by flame spray pyrolysis (FSP) of zinc acetate (ZA) and either hexamethyldisiloxane (HMDSO) or SiO2-sol dispersed in either methanol or a water-in-oil emulsion. The product particles were characterized by nitrogen adsorption, infrared absorption and X-ray diffraction. The evolution of solid or hollow particle formation along the flame axis was elu...