where the peak shapes were described by a pseudo-Voigt function and the background was modeled with an 6-term polynomial. Additionally, the PXRD patterns obtained at room temperature and 100 K were analyzed by Le Bail refinement using the GSAS and EXPGUI software, 2,3 where the peak shapes were described by a pseudo-Voigt function (CW profile function 3) and the background was modeled with an 4...

Objective: Aim of this present study was to prepare and characterize the different polymorphs of Prulifloxacin using Powder X-Ray Diffraction analysis (PXRD), Scanning Electron Microscopy (SEM), Differential Scanning Calorimetry (DSC), Fourier Transform Infrared Spectrometry (FTIR) and dissolution studies. Methods: Polymorphs of Prulifloxacin were prepared by cooling crystallization method usin...

In this study, a novel ternary complex system (TCS) composed of baicalein, phospholipids, and Soluplus was prepared to improve the flowability and dissolution for baicalein phospholipid complex (BPC). TCS was characterized using differential scanning calorimetry (DSC), infrared spectroscopy (IR), powder X-ray diffraction (PXRD), and scanning electron microscopy (SEM). The flowability, solubilit...

Preparation of good quality magnesium oxide from seawater is the most challenging job because vast majority undesired impurities come during precipitation stage. Hence, double salt route has been developed as a very unique technique to prepare refractory grade seawater. Controlled addition carrier reagent at precipitating stage precipitates salt. The transformed carbonate (MgCO3), which after c...

Department of Chemistry, Massachusetts 02139, USA. E-mail: [email protected] Department of Materials, Imperial College Department of Materials Science and Engi South Korea † Electronic supplementary information PXRD patterns, IR spectra, table of elec energies, current density vs. electrical curves at various temperatures, tem conductivity, Fe Mössbauer spectra, ma area analysis, table of various ...

Instituto de Tecnoloǵıa Qúımica (UPV-CSIC Consejo Superior de Investigaciones Cien Valencia, Spain. E-mail: [email protected] Berzelii Center EXSELENT on Porous M Chemistry, Department of Materials and University, SE-106 91 Stockholm, Sweden. E † Electronic supplementary information determination by RED, separation usin renement against PXRD of as-made an textural properties, Si and F solid st...