Starting from readily available 2-substituted-4-methylthiazole-5-carboxylic acid hydrazide (1), The title compounds were prepared. The reaction of compound 1 (R=CH3) with formic acid yielded 1-(formyl)-2-(2,4-dimethylthiazole-5-carboxyl) hydrazine (2). Refluxing the latter with phosphorous pentasulfide in xylene afforded compound 3, the reaction of compound 2 with phosphorous pen...

shrink fit process is a useful technique in order to introduce beneficial residual stress in compound pressure vessels. in this paper, the effects of geometrical tolerances on residual stresses have been studied for a compound shrink fitted pressure vessel, practically. three layers, which are designed based on an optimum nominal thickness and overlap dimensions and tolerances, have been fitted...

this research work is devoted to experimental and theoretical evaluations of a hybrid constitutive model which was designed to simulate the mechanical behavior of a tread rubber compound. the model is a combination of yeoh hyperelastic model with a strain-rate hysteresis model developed by bergstrom and boyce. the parameters of the yeoh model were calibrated from experimental data of the astm d...

reaction of aryl methyl ketone with isatin in the presence of a base afforded 2- arylquinoline-4-carboxylic acid (3). reaction of diazomethane with compound 3 yielded the ester 4. compound 5 was prepared from the reaction of n, n'-dialkylethyl (or propyl) arnine with 4. addition of hydrazine hydrate to compound 4a gave 2- (2- pyridyl) quinoline-4-carboxylic acid hydrazide (6). reaction of ...

This paper puts forward a verification method for compound purposes and compound reasons to be used during purpose limitation. When it is absolutely necessary to collect privacy related information, it is essential that privacy enhancing technologies (PETs) protect access to data – in general accomplished by using the concept of purposes bound to data. Compound purposes and reasons are an enhan...

the conformational behaviors of 2,3-bis(methylthio)-1,4-dioxane (1), 2,3-bis(methylthio)-1,4-dithiane (2) and 2,3-bis(methylthio)-1,4-diselenane (3) have been analyzed by means ofhybrid-density functional theory (b3lyp/def2-tzvpp) based method and nbo interpretation.b3lyp/def2-tzvpp results showed that the axial conformations of compounds 1-3 are morestable than their equatorial conformations. ...

[reaction: see text] A novel type of photo-protecting group for carbonyl compounds is described. The protecting group is readily accessed in one step from commercially available material. Installation of the protecting group upon the carbonyl compounds is achieved in excellent yields. The carbonyl compounds in their protected form are remarkably stable under various conditions and can be releas...