Abstract Novel bulk single-component sulfide catalysts were prepared under the conditions of solid-phase dispersion МoS 2 molybdenite at various mechanical treatment times and amounts polar nonpolar liquid microadditives. The chemical degradation samples in air was found to lead formation surface sulfate anions that shield catalytically active Mo sites. Indirect correlations hydrodesulfurizatio...

highly sinterable alumina nano-powders have been synthesized by a sol-gel combustion method with glycine asfuel. the preparation involved the thermal decomposition of a chelating agent (fuel)-nitrate gel and theformation of amorphous precursors. the nanopowders calcined at 1100°c were characterized by x-ray powderdiffraction (xrd) and scanning electron microscopy (sem). it was found that the ch...

the nanopowders of sno2, casno3 and ca2sno4 in the size rang of 5-70 nm have been prepared using solid-state reaction technique. the technique is convenient and inexpensive in comparison to the conventional routes of compound prepared and processing where, many steps of mixing and annealing are involved. formation of resultant compounds was explained on the basis of reaction taken place between...

Low-temperature aqueous chemical growth methods have shown great potential in the synthesis of ZnO nanostructures. Hexamethylenetetramine (HMTA) is the most common chemical substance used in the hydrothermal synthesis. In this study zinc oxide nanoparticles were prepared via hydrothermal growth using zinc acetate dihydrate and sodium hydroxide, as precursors instead of HMTA, as it is commercial...

Fe-based nanoparticles were prepared by laser-driven pyrolysis. The assynthesised powder consists of α-Fe and Fe3O4/γ-Fe2O3 nanoparticles embedded in a pyrolytic carbon matrix. The crystallite size of 1.8 nm for α-Fe was calculated using the Scherrer formula. The as-synthesised nanopowder was superparamagnetic. The maximum of the zero-field cooling curve was observed at 32 K and the distributio...

A hierarchically organized Co3O4 nanopowder was obtained via programmed chemical precipitation, exhibiting several levels of microstructural self-organization: the initial particles are 40 ± 5 nm in size (average CSR is 32 3 nm), have a somewhat distorted rounded shape and combined into curved chains, which, turn, form flat agglomerates approximately 350 50 diameter. The thermal behavior semipr...