The structural evolution of a Zr64.13Cu15.75Ni10.12Al10 metallic glass is investigated in-situ by high-energy synchrotron X-ray radiation upon heating up to crystallization. The structural rearrangements on the atomic scale during the heating process are analysed as a function of temperature, focusing on shift of the peaks of the structure factor in reciprocal space and the pair distribution fu...

Periodic arrays of micrometer-sized ferromagnetic structures with perpendicular magnetic anisotropy are prepared by nanoindentation at the surface of a Fe(67.7)B(20)Cr(12)Nb(0.3) glassy ribbon initially showing in-plane magnetic anisotropy. The indented regions exhibit enhanced coercivity and saturation magnetization with respect to the surrounding nondeformed matrix. These effects are due to a...

It is known that nanocrystallites can form in shear bands produced during severe bending or high-energy ball milling of thin ribbons of a metallic glass. We present direct experimental evidence that highly confined and controlled local contact at the ultrafine scale in the form of quasi-static nanoindentation of a bulk glassy metal alloy at room temperature can also cause nanocrystallization. A...

To understand the effect of substrate microstructure on the formation of TiO2 nanotubes, anodic oxidizations of commercially pure titanium subjected to surface mechanical attrition treatment (SMATed-Ti) and unSMATed-Ti in a glycol solution containing NH4F and small amounts of water were investigated. The SMATed-Ti exhibit a nanocrystallized surface layer containing a high density of grain bound...

Ultrasonic peening treatment (UPT) as a method of severe plastic deformation was used to treat cruciform welded joints of Q345 steel. The application of UPT achieves material surface nanocrystallization of the peening zone, reduces stress concentration, and produces residual compressive stresses at the welded toe. Micro-structure, hardness, stress relief, S-N curve, and the fatigue fracture mec...

We have studied the phase and structure evolution of the Ti33Cu67 amorphous alloy subjected to electrical pulses of high current density. By varying the pulse parameters, different stages of crystallization could be observed in the samples. Partial polymorphic nanocrystallization resulting in the formation of 5- to 8-nm crystallites of the TiCu2 intermetallic in the residual amorphous matrix oc...