Dry (mechanochemical) synthesis of Y(BH4)3. For mechanochemical synthesis the vibrating mill (Testchem) and chromium steel bowl and disc were used. Substrates, YCl3 and LiBH4 were mixed in ca 1:3 molar ratio (with a 5 % excess of MBH4) and milled for ca. 60 minutes in Ar atmosphere. Milling periods of 3–5 minutes were altered with 2–5 minutes rests to avoid thermal decomposition of the products...

Solid solutions of BiFeO 3 and BaTiO are promising lead-free piezoelectric materials, especially around the morphotropic phase boundary at 0.67BiFeO -0.33BaTiO . Still, these materials challenged by instability limited understanding processing-properties relationship. Here, we investigate mechanochemical activation use as seed particles for phase. Contrary to expectations from seeding in lead-b...

ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 complex was prepared according to literature report. the reaction between aforementioned complex via sodium alkoxides as a reactants, were carried out in the solid state. the [ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 undergoes an intramolecular two electrons oxidation-reduction reaction at room temperature and metallic nickel nanoparticles (ni1-ni5) was ...

ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 complex was prepared according to literature report. the reaction between aforementioned complex via sodium alkoxides as a reactants, were carried out in the solid state. the [ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 undergoes an intramolecular two electrons oxidation-reduction reaction at room temperature and metallic nickel nanoparticles (ni1-ni5) was ...

in this work, the strontium-doped lanthanum manganite- a ceramic material- used as cathode in solid oxide fuel cells. an impression of grinding time on the structural and thermal properties of sr-doped lamno3 system with la1-xsrxmno3 (x=0.2) stoichiometric ratio was investigated. the nano crystallite lsm powder with cubic structure was prepared by varying the milling time of planetary monomill ...

Highly conductive, transparent, flexible and scalable graphene hybrid thin films with controlled domain size were successfully fabricated via a mechanochemical method, screen printing and pressure-assisted reduction process.

Strong and stable under tension? In this review we present the recent efforts investigating the mechanochemical properties of interlocked structures by atomic force microscopy and polymer mechanochemistry.

In this work, the strontium-doped lanthanum manganite- a ceramic material- used as cathode in solid oxide fuel cells. An impression of grinding time on the structural and thermal properties of Sr-doped LaMnO3 system with La1-xSrxMnO3 (x=0.2) stoichiometric ratio was investigated. The nano crystallite LSM powder with cubic structure was prepared by varying the milling time of planetary monomill ...