نتایج جستجو برای: hydrazide
تعداد نتایج: 1486 فیلتر نتایج به سال:
In the title compound, C(16)H(17)N(3)O(2)·0.5H(2)O, the two hydrazide mol-ecules are approximately planar: the dihedral angles between the two substituted benzene rings are 7.7 (2) and 4.2 (2)°. Both hydrazone mol-ecules exist in a trans geometry with respect to their methyl-idene units. In the crystal, the water mol-ecule lies between the two organic mol-ecules and makes bifurcated O-H⋯(N,O) h...
Tobacco mainstream smoke (MSS) and sidestream smoke (SSS), butts, and ashes from commercial cigarettes and maleic hydrazide (MH) spiked cigarettes were analyzed for their MH contents. The MH transfer rates obtained for MSS ranged from 1.4% to 3.7%, for SSS ranged from 0.2% to 0.9%, and for butts ranged from 1.1% to 1.9%. And as expected, MH is absent in ashes. The transfer rate of MH into mains...
Z. Naturforsch. 61b, 431 – 436 (2006); received January 17, 2006 The 3,4-substituted 2-oxo-piperazines 5 – 9 are obtained by [3+2] cycloaddition from nitrone 1 and a variety of alkenes. Subsequent functionalization of the bicyclic adducts involves reductive N-O bond cleavage. A route towards libraries of immobilized 1,3-aminoalcohols with a 3,4-substituted 2-oxo-piperazine scaffold is briefly d...
Three hydrazide-based Schiff bases have been synthesized and characterized by IR, UV-vis X-ray diffraction methods. A detail analysis of intermolecular interactions has performed Hirshfeld surface DFT calculations.
In the title compound, C14H13N3O2·2H2O, the hydrazone mol-ecule adopts an E conformation with respect to the C=N bond. The dihedral angle between the benzene and pyridine rings is 8.55 (10)°. The methyl-idene-hydrazide [-C(=O)-N-N=C-] fragment is essentially planar, with a maximum deviation of 0.0375 (13) Å. The mean planes of the benzene and pyridine rings make dihedral angles of 2.71 (14) and...
Starting from readily available 2-substituted-4-methylthiazole-5-carboxylic acid hydrazide (1), The title compounds were prepared. The reaction of compound 1 (R=CH3) with formic acid yielded 1-(formyl)-2-(2,4-dimethylthiazole-5-carboxyl) hydrazine (2). Refluxing the latter with phosphorous pentasulfide in xylene afforded compound 3, the reaction of compound 2 with phosphorous pen...
Inhibitors of soluble epoxide hydrolase (sEH) represent one of the novel pharmaceutical approaches for treating hypertension, vascular inflammation, pain and other cardiovascular related diseases. Most of the potent sEH inhibitors reported in literature often suffer from poor solubility and bioavailability. Toward improving pharmacokinetic profile beside favorable potency, two series of 4-benza...
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