The structure, chemistry, and spatial distribution of Mn-bearing nanoparticles dissolved from the Li1.05Mn2O4 cathode during accelerated electrochemical cycling tests at 55 °C and deposited within the solid electrolyte interphase (SEI) are directly characterized through HRTEM imaging and XPS. Here we use air protection and vacuum transfer systems to transport cycled electrodes for imaging and a...

Quantifying and characterising atomic defects in nanocrystals is difficult and low-throughput using the existing methods such as high resolution transmission electron microscopy (HRTEM). In this article, using a defocused wide-field optical imaging technique, we demonstrate that a single ultrahigh-piezoelectric ZnO nanorod contains a single defect site. We model the observed dipole-emission pat...

The important role of surface sensitive characterization techniques such as Auger electron spectroscopy (AES), X-ray photo electron spectroscopy (XPS), time of flight scanning ion mass spectrometry (TOF-SIMS) and High resolution transmission electron microscopy (HRTEM) for the characterization of different phosphor materials is discussed in this short review by giving selective examples from pr...

S1. Translational motion of 1D sulfur chains inside SWCNT Fig. S1 shows the observed translational motion of encapsulated sulfur chains during the HRTEM measurements. In the initial stage of the HRTEM observation, we find two lines inside the nanotube that extend across the entire SWCNT length (Fig. S1A). In subsequent observations taken several tens of seconds later (Fig. S1B), the length of t...

Partially sericitized tourmaline from a pegmatite was investigated using high-resolution transmission electron microscopy (HRTEM). Fine-grained muscovite crystals form extensive narrow veinlets preferentially developed along the {110} and {100} cleavages of tourmaline, indicating that a cleavage-controlled alteration mechanism was dominant. HRTEM images show that tourmaline-muscovite interfaces...

Transformation of Al(NO3)3∙9H2O (upon heating in the range of 20-1200 °C) into blends of amorphous and crystalline boehmite (210-525 °C), amorphous alumina and crystalline γ-Al2O3 (850 °C), and crystalline α-Al2O3 (1100 °C) was analyzed using X-ray diffraction (XRD), high-resolution transmission electron microscope (HRTEM), infrared (IR) spectroscopy, thermogravimetry, and low-temperature nitro...

Atomically resolved imaging of organic molecules consisting of thin crystals by aberration-corrected (AC) HRTEM was studied by experimental observations and image simulations. An atomically resolved image of the hexadecachlorophthalocyanatocopper (CuPcCl16) molecule was obtained under low-dose conditions. The conditions for imaging organic frameworks were found to be more restricted than those ...

SnO(2)/Sn nanocables have been grown on single-crystal Si substrates by metal catalyst assisted thermal evaporation of SnO powders. The morphologies and structures of the prepared nanocables were determined on the basis of field emission scanning electron microscopy (FESEM), high-resolution transmission electron microscopy (HRTEM), x-ray diffraction (XRD), Raman and photoluminescence (PL) spect...