It is generally supposed that the preconcentration procedure is used for the determination of metal concentrations under the sensitivity of the measurement method. This study showed that preconcentration is also need for the beryllium (Be) concentration over the sensitivity of atomic absorption spectrometry. For this purpose, a simple and selective method for the determination of Be in solid sa...

The atomic absorption of aluminum with air-acetylene flame was interfered by the formation of involatile compounds in the flame. Amines promoted the atomization of aluminum in the flame. Aluminum could be determined by atomic absorption spectrometry with an air-acetylene flame. The absorption of aluminum increased and then attained a constant value as the concentration of amines increased. The ...

A novel analytical method for accurate determination of boron (B), phosphorous (P), and molybdenum (Mo) content in biosludge samples based on a relatively recent analytical technique, microwave plasma atomic emission spectrometry (MP-AES), is developed in the present work. Microwave assisted acid digestion method is utilized to extract B, P, and Mo from biosludge. To demonstrate the reliability...

Atomic Absorption Based Techniques. Atomic Fluorescence Spectroscopy. Figure 1.3 Schematic diagram showing the before (left) and after (right) the draw the sample into a nebulizer by the Bernoulli Effect where it is converted. Atomic absorption and emission spectroscopy in the ultraviolet and visible A schematic diagram of a UV-Vis spectrophotometer is shown in Figure.11. Preface Inductively co...

Abstract This work reports a simple and sensitive on-line solid-phase extraction system for the pre-concentration determination of trace amount Co(II (ions by flame atomic absorption spectrometry (FAAS). method is based on retention cobalt ions with polyvinyl chloride modified 3-(2-thiazolylazo)-2,6-diaminopyridine in mini-column system. The retained Co(II) were eluted 1.0 mol L −1 HCl, direct ...

The aim of this study was to determine and compare the concentration of copper (Cu) in liver and muscle of two fish species Squalius cephalus and Capoeta capoeta gracilis. The fish were caught in four sampling sites along Tajan River, Mazandaran Province, northern Iran. The concentration of Cu was determined using flame atomic absorption spectrometry. There were significant differences (P

background: nickel is an important constituents widely used in different industrial processes for production of various syn¬thetic materials. for evaluation of workers’ exposure to trace toxic metal of ni (ii), environmental and biological monitor¬ing are essential processes, in which, preparation of samples is one of the most time-consuming and error-prone as¬pects prior to analysis. methods: ...

A new method for the determination of trace copper(II) in food samples by Cloud Point Extraction(CPE) combined with Flame Atomic Absorption Spectrometry(FAAS) is presented and evaluated. The method is based on the fact that hydrophobic complex of copper(II) with sodium diethyldithiocarbamate (DDTC) was formed at pH 6.0 and subsequently the hydrophobic complex was extracted into surfactant-r...

The main scope of this paper is first of all to verify the efficiency of the flame atomic absorption spectroscopy (FAAS) method for analysis of some trace elements in extracts of fractionation analysis of the gravitation dust sediments. Investigation was oriented to the analysis of some markedly toxic trace elements in the extracts of gravitation dust sediments as well as on efficiency evaluati...

Background: cold-induced aggregation micro extraction based (CIAME) based on ionic liquid was used as a rapid and simple method for determination trace amounts of cadmium and lead in milk powder by analysis with flame atomic absorption spectrometry (FAAS). Methods: Sample solution containing of Cd2+ and Pb2+ in dynamic range, phosphate buffer (pH = 9, 3 ml), diethyl dithiocarbamate (complexin...