Ground fish scales were characterized as a solid phase extraction medium for preconcentration of parts per billion levels of transition elements prior to their flame atomic absorption spectroscopic (FAAS) determination. At the indicated optimum pH, sorption follows the order Cd (pH 7.0) ≥ Pb (pH 5.5)> Fe (pH 4.8) > Cu > Zn (pH 6.0) > Ni (pH 7.5) > Mn (pH 8.5) > Cr (pH 4.8). At pH 5.5, following...

Correct use of instruments and irrigating solutions are major factors during chemo-mechanical preparation of root canals. Ultrasonically activated files and solutions are used for debridement of canals. In this study 42 single rooted anterior human teeth were used. The roots were divided into two groups. One group received an application of 17% ethylenediamine tetra acetic acid (EDTA) of 1 ml f...

BACKGROUND Compounds containing ethylenediamine (-NCH2CH2N-) moiety are known to exhibit antimicrobial, -fungal, -bacterial, -tuberculosis and -cancer activities. MATERIALS AND METHODS In the present study, we evaluated the in vitro cytotoxic activity of N,N'-bis(2-hydroxybenzyl)- (6), N,N'-bis(5-bromo-2-hydroxybenzyl)- (7) and N,N'-bis(5-chloro-2-hydroxybenzyl) (8)- ethylenediamine dihydroch...

Four new ethylenediamine-templated iron arsenates and fluoroarsenates have been hydrothermally synthesized from iron metal, hydrofluoric and arsenic acids, and ethylenediamine. Fe(H2AsO4)(HAsO4)2.enH2.H2O (1) is one-dimensional and contains chains, FeIIIFeIIF2(HAsO4)(AsO4).enH2.2H2O (2) is a layered fluoroarsenate, and Fe3(HAsO4)6.enH2.NH3.NH4 (3) and Fe2F2(AsO4)2(H2O).enH2 (4) are an arsenate ...

INTRODUCTION This study aimed to compare the efficacy of MTAD, Glyde and EDTA in removing the post-preparation smear layer and debris produced in apical third of curved molar root canals. MATERIALS AND METHODS Forty extracted human maxillary first molars with curved mesiobuccal canals (30˚-35˚), similar root lengths and morphologies were divided into 3 experimental groups (n=12) and one contr...

Various authors have reported methods for the colorimetric estimation of alpha-amino nitrogen with ninhydrin (Moore and Stein, 1948, 1954; Smith and Agiza, 1951 ; Troll and Cannan, 1953; Yemm and Cocking, 1955; Kalant, 1956; Rosen, 1957). Only Kalant has applied this method to the direct measurement of alpha-amino nitrogen in biological fluids; he reported on the determination of total alpha-am...

Antioxidant activity of Peucedanum pastinacifolium Boiss. & Hausskn aerial part hydroalcoholic extract (HAE) and polyphenolic extract (PPE) as well as their total phenolic and flavonoid contents were studied. Phenolic and flavonoid contents were respectively estimated as gallic acid and quercetin equivalents. The in vitro antioxidant activity of two extracts of P. pastinacifolium were evaluated...

Pseudothrombocytopenia remains a challenge in the haematological laboratory. The pre-analytical problem that platelets tend to easily aggregate in vitro, giving rise to lower platelet counts, has been known since ethylenediamine-tetra acetic acid EDTA and automated platelet counting procedures were introduced in the haematological laboratory. Different approaches to avoid the time and temperatu...

To investigate the effects of calcium disodium ethylenediamine tetra-acetate (CaEDTA) on the urinary excretion, erythrocyte, and plasma concentrations and exposure indicators of seven heavy metals, CaEDTA was administered by intravenous infusion to 20 workers exposed to lead, zinc, and copper. The workers' blood lead concentrations ranged from 22 to 59 micrograms/dl (mean 38 micrograms/dl (1.8 ...

BACKGROUND AND AIMS The aim of the present study was to compare 1.3% sodium hypochlorite (NaOCl) in MTAD (mixture of tetracycline isomer, acid, and detergent) for the removal of the smear layer and induction of canal erosion. MATERIALS AND METHODS 38 maxillary incisors were divided in three experimental groups of 10 and two positive and negative control groups of each 4 teeth, and prepared us...