The paper reports a process for synthesis of γ-alumina from kaolin. Kaolin was transformed to meta-kaolin by calcination at 800 ̊C for 2h. γ-alumina powder was synthesized through extracting alumina from metakaolin via H2SO4 and meta-kaolin reactions and consequently precipitation in ethanol, which led to form the aluminum sulfate. The precipitated aluminum sulfate was dried and calcined at 900 ̊...

Many pioneers from around the world followed this initial experience but long-term results and good methodology were lacking. Recently, a number of reports 4-6 have focused attention again on an alumina-on-alumina combination. More than 30 years after its introduction into clinical practice, this article considers the current information on the alumina-on-alumina combination from both experimen...

OBJECTIVES The objective of the present study was to analyze the superficial roughness and the interface between enamel and composite resin restorations after dental bleaching procedure. MATERIALS AND METHODS Black's class V cavities were made and restored with composite resin, and the whole set, enamel-restorative material, was treated with 35% hydrogen peroxide. Seven procedures of 30 min e...

The aim of this study was to detect and quantify the main residual monomers released from composites, using high performance liquid chromatography (HPLC). Discs were made with dental composites (Herculite XRV, Tetric Ceram and Filtek Z250) and immersed in deionized water at 37°C for 28 days, with water changes in 1, 7, 14 and 21 days. The mean concentration of residual monomers were subject to ...

A new rapid, very simple and one-step sol-gel strategy for the large-scale preparation of highly porous γ-Al₂O₃ is presented. The resulting mesoporous alumina materials feature high surface areas (400 m² g-1), large pore volumes (0.8 mL g-1) and the γ-Al₂O₃ phase is obtained at low temperature (500 °C). The main advantages and drawbacks of different preparations of mesoporous alumina materials ...

Monolithic ceramics have been fabricated from coated green fibers to create fibrous microstructures. The fibrous monoliths consist of high aspect ratio polycrystalline regions (cells) of a primary phase separated by thin secondphase regions (cell boundaries) designed to improve fracture resistance. The cells are the remnants of the green fiber which consists of ceramic powder and a polymer bind...

Thin alumina films have found applications in electronic circuits and cutting tools and have been recently explored as protective coatings against high temperature oxidation, but these studies have been relatively rare. In this study, amorphous alumina films 3.5 pm thick were produced by reactive sputtering on Co-30Cr-6Al-0.5Y coatings, using a pure aluminum target in Ar + 0 2 atmosphere. Isoth...

The paper reviews progress for a program of research on alumina ceramics processing, with particular reference to diffraction results achieved using tube x-rays, neutrons and synchrotron radiation. Outcomes from three related studies are examined. l Calcination of alumina hydrates to o-alumina via intermediate aluminas, including some new results indicating the co-existence of cubic and tetrago...

An efficient and green protocol for the synthesis of αaminonitriles derivatives by one-pot reaction of different aldehydes with amines and trimethylsilyl cyanides has been developed using natural alumina, alumina sulfuric acid (ASA), nano-γ-alumina, nanoalumina sulfuric acid (nano-ASA) under microwave irradiation and solvent-free conditions. The advantages of methods are short reaction times, h...