نتایج جستجو برای: bjh

تعداد نتایج: 275  

Farzad Zamani Roozbeh Kalbasi, Zohreh Shahzeidi

A simple and green synthetic strategy to prepare BaO/TiO2-ZrO2 as a solid base catalyst was reported. These materials with various amounts of BaO were prepared by the adsorption method. The physical and chemical properties of BaO/TiO2-ZrO2 were investigated by X-ray diffraction, X-ray fluorescence, specific surface area and BJH pore size distribution, FT-IR spectroscopy, scanning electron micro...

2015
Carmen Cavallo Alberto Salleo Daniele Gozzi Francesco Di Pascasio Simone Quaranta Riccardo Panetta Alessandro Latini

Solid solutions of the rare earth (RE) cations Pr(3+), Nd(3+), Sm(3+), Gd(3+), Er(3+) and Yb(3+) in anatase TiO2 have been synthesized as mesoporous beads in the concentration range 0.1-0.3% of metal atoms. The solid solutions were have been characterized by XRD, SEM, diffuse reflectance UV-Vis spectroscopy, BET and BJH surface analysis. All the solid solutions possess high specific surface are...

Journal: :Molecules 2016
Smaail Radi Said Tighadouini Maryse Bacquet Stephanie Degoutin Jean-Philippe Dacquin Driss Eddike Monique Tillard Yahia N Mabkhot

Molecules bearing β-keto-enol functionality are potential candidates for coordination chemistry. Reported herein is the first synthesis and use of a novel designed ligand based on β-keto-enol group embedded with pyridine and thiophene moieties. The product was prepared in a one-step procedure by mixed Claisen condensation and was characterized by EA, m/z, FT-IR, (¹H, (13)C) NMR and single-cryst...

2012
Yongqiang Wen Liping Xu Chuan bao Li Hongwu Du Linfeng Chen Bin Su Zhiliang Zhang Xueji Zhang Yanlin Song

Tetraethoxysilane (TEOS, 28%), n-cetyltrimethylammonium bromide (CTAB, ≥99%), ammonium hydroxide solution (25%), 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide (EDC, 99%), N-Hydroxysuccinimide (NHS, 98%), 3-Aminopropyltriethoxy-silane (APTES, 99%), succinic anhydride (99%), sodium citrate tribasic dihydrate, tannic acid, and Rhodamine B were purchased from Sigma Company. Hydrogen tetrachloroaur...

2012
S. Rajeswaran S. Rajasekaran

As traffic demand on road networks steadily increases every year, the need for alleviation of global congestion arises. Our contribution lies in assisting of traffic engineers and policy makers who are faced with the problem of controlling the traffic flows. In this paper, we explore the usefulness of cellular automata to traffic flow modeling. We extend some of the existing CA models to captur...

2017
Yan Bao Tong Wang Qiaoling Kang Chunhua Shi Jianzhong Ma

Hollow silica spheres (HSS) with special interior spaces, high specific surface area and excellent adsorption and permeability performance were synthesized via micelle-template method using cetyl trimethyl ammonium bromide (CTAB) micelles as soft template and tetraethoxysilane (TEOS) as silica precursor. SEM, TEM, FT-IR, XRD, DLS and BET-BJH were carried out to characterize the morphology and s...

2011
Wen Jie Guo Wen-Jie Guo Yan Wang Ming-Zhi Huang Jin-Quan Wan Yong-Wen Ma

Variation in the pore structure of eucalyptus fibre during recycling was investigated using low-temperature nitrogen adsorption, atomic force microscopy (AFM), and fractal geometry. The BrunauerEmmett-Teller (BET) surface area of the fibre fell to 55.1% of the original value after the first cycle, and to 49.0% after the second cycle, ultimately declining to 35.0% after the fourth. The Barret-Jo...

2013
Muggundha Raoov Sharifah Mohamad Mhd Radzi Abas

β-Cyclodextrin-ionic liquid polymer (CD-ILP) was first synthesized by functionalized β-cyclodextrin (CD) with 1-benzylimidazole (BIM) to form monofunctionalized CD (βCD-BIMOTs) and was further polymerized using a toluene diisocyanate (TDI) linker to form insoluble CD-ILP (βCD-BIMOTs-TDI). The βCD-BIMOTs-TDI polymer was characterized using various tools and the results obtained were compared wit...

2004
P Laguna

W e present here a QT database designed j b r evaluation of algorithms that detect waveform boundaries in the EGG. T h e dataabase consists of 105 fifteen-minute excerpts of twochannel ECG Holter recordings, chosen to include a broad variety of QRS and STT morphologies. Waveform bounda,ries f o r a subset of beats in, these recordings have been manually determined by expert annotators using a n...

Journal: :Journal of colloid and interface science 2007
Xiu-Wen Wu Hong-Wen Ma Jin-Hong Li Jun Zhang Zhi-Hong Li

An economical mesoporous aluminosilicate was synthesized with microcline as starting material and the precursor 13X zeolite as seed for crystal structure on mesoporous walls. In this method, a mixture of microcline and Na2CO3 with a molar ratio of 1:1.05 was first calcined at 1093 K for 2.5 h. The calcined materials were mixed with 35 ml C16TMABr aqueous solution (containing 8.2 g C16TMABr) and...

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