In this study, new compounds of Schiff bases were prepared (1-6), from the reaction sulfamethoxazole with benzaldehyde derivatives. (1-6) converted to 1,3-Oxazepine-4,7-dione and 1,3-Benzooxazepine-4,7-dione derivatives (7-18) through maleic anhydride as well phthalic using crushing, grinding microwave irradiation method. The structures all have been identified by (I.R) technique, also some (1H...