نتایج جستجو برای: x ray powder diffraction xrd

تعداد نتایج: 737007  

Journal: :journal of physical & theoretical chemistry 2009
. thanasanvorakun pongsri mangkomtong majid monajjemi nikom sangkorntong

sn02 nanowires with diameters of 30 — 200 nm have been synthesized by using carbothermalprocess via a thick film of tin dioxide and carbon powder precursor. the nanowires werecharacterized by x-ray power diffraction (xrd), scanning electron microscopy (sem),transmission electron microscopy (tem) and selected area electron diffraction (saed).the gas sensing characteristic of nanowires toward eth...

Journal: :Journal of Synthetic Organic Chemistry, Japan 1962

درودیان, مسعود, طیبی فرد, سید علی , یزدانی راد, رحیم, احمدی, کامران,

X-ray powder diffraction data for Mo2.85Al1.91Si4.81 are presented here. The new Mo2.85Al1.91Si4.81 compound was successfully prepared, using the self-propagating high-temperature synthesis (SHS) technique. The starting atomic mixture of reactant powders was Mo + 2(1 - x)Si + 2xAl with 0.2 ≤ x ≤ 0.5. The final powder compound obtained by the SHS technique was determined to be in x = 0.2; Mo(Si,...

2006
G. Liang Z. Tang H. Fang K. Salama

To clarify the inconsistency between calculated and existing experimental X-ray diffraction (XRD) pattern for dicopper magnesium (MgCu2) nd to identify the impurity phase in Cu-sheathed MgB2 superconductors, polycrystalline MgCu2 samples were synthesized and studied by XRD easurement. The XRD result shows that the (2 2 0), (4 2 2), (6 2 0), and (6 4 2) reflection lines, which are missing from t...

2017
Woon Bae Park Jiyong Chung Jaeyoung Jung Keemin Sohn Satendra Pal Singh Myoungho Pyo Namsoo Shin Kee-Sun Sohn

A deep machine-learning technique based on a convolutional neural network (CNN) is introduced. It has been used for the classification of powder X-ray diffraction (XRD) patterns in terms of crystal system, extinction group and space group. About 150 000 powder XRD patterns were collected and used as input for the CNN with no handcrafted engineering involved, and thereby an appropriate CNN archi...

Journal: :Proceedings of the National Academy of Sciences of the United States of America 2011
Reza Mohammadi Andrew T Lech Miao Xie Beth E Weaver Michael T Yeung Sarah H Tolbert Richard B Kaner

Tungsten tetraboride (WB(4)) is an interesting candidate as a less expensive member of the growing group of superhard transition metal borides. WB(4) was successfully synthesized by arc melting from the elements. Characterization using powder X-ray diffraction (XRD) and energy-dispersive X-ray spectroscopy (EDX) indicates that the as-synthesized material is phase pure. The zero-pressure bulk mo...

2014
Yashavanth Kumar H. S. Bhojya Naik A. S. Roy K. N. Harish R. Viswanath

ZnFe2O4 nanocomposites have been prepared by a simple co‐precipitation method. The prepared samples were characterized by Scanning Electron Microscopy (SEM), Powder X‐ray Diffraction (XRD), Energy Disperse X‐ray Analysis (EDX), Transmission electron microscopy (TEM) and UV‐visible absorption spectral techniques. Conductivity measurements show a transition from ferrimagnetism to...

Journal: :Indian journal of biochemistry & biophysics 2014
Vimal S Joshi Sonal R Vasant J G Bhatt Mihir J Joshi

Urinary calculi constitute one of the oldest afflictions of humans as well as animals, which are occurring globally. The calculi vary in shape, size and composition, which influence their clinical course. They are usually of the mixed-type with varying percentages of the ingredients. In medical management of urinary calculi, either the nature of calculi is to be known or the exact composition o...

بخشی, سعیدرضا, برهانی, غلامحسین, خواجه لکزای, محمد,

In this study, synthesis of silicon nitride by mechanical alloying and the effects of important parameters of milling time and heat treatment temperature, time and rate are presented. Silicon micro powder and nitrogen gas were used as precursor materials. Synthesized phases, morphology and particle size were investigated by X-ray diffraction pattern (XRD) and Field emission scanning electron mi...

2004
Dennis W. Smithenry Kenneth S. Suslick

A review of the recent literature is presented which assesses the development of robust microporous porphyrin framework solids and their potential to perform selective sorption or heterogeneous shapeor size-selective catalysis. The review focuses only on those porphyrin solids whose porosity is robust, i.e. whose framework remains after the removal of solvates, as determined by thermal gravimet...

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