Three solid-solid and two solid-liquid diffusion couples together with 32 key samples were used to construct the isothermal section of the Mg-Ni-Y system at 673 K. The present investigation revealed 12 ternary intermetallic compounds. Crystal structures of two ternary compounds τ1 (Gd4RhIn prototype with lattice parameter of a = 1.3666 nm) and τ2 (Mo2FeB2 prototype with lattice parameters of a ...

X-ray diffraction is a commonly used experimental technique for identifying the structure of crystalline materials[3]. A crystalline material has its atoms arranged in periodic lattices with long-range symmetry. As a result, it scatters a beam of X-rays in well-defined patterns. Analysis of an X-ray diffraction pattern produced by a material yields extensive information about the structure of t...

in this study, a feasible green method for the synthesis of copper oxide nanocrystalline is described by using sour cherry juice which has a significant effect on crystalline size, and morphology. the benefits of the green method, not only nanometer scale are formed but also low-cost method are obtained in a normal atmosphere which it has been used (ch3coo)2cu.h2o individually as cu sources. al...

according to circumstance of kerman sarcheshmeh cooper complex that its anode slime is mainly consisted of cu, ag, au, pb and se. in this work, recovery of silver from anode slime and subsequent synthesis of silver nanoparticles from leaching solution was made. silver was separated from anode slime by using of hno3 and hcl. x-ray fluorescence spectroscopy (xrf) was used to characterize anode sl...

The nanocrystallization of Co67Fe4Cr7Si8B14 amorphous ribbons which prepared by planar flow melt spinning process (PFMS) was investigated. Crystallization of the ribbons was studied by differential thermal analysis (DTA), X-ray diffraction (XRD) and transmission electron microscopy (TEM). The DTA result of amorphous ribbon at heating rate of 10˚C/min showedoccurrence of phase transitions in two...

here we present our experimental results in synthesizing au-cu nano-particles with tunable localized surface plasmon resonance frequency through wet-chemical at temperature room. the reaction is performed in the presence of ascorbic acid as a reducing agent and polyvinyl pyrrolidone as capping agent via four different procedures: (1) mixture of 90% haucl4 and 10% cuso4.5h2o precursors, (2) mixt...

Several techniques have been utilized for the preparation of hydroxyapatite (HA) and other calcium phosphates for the development of biomaterials. It is vital to know the reaction kinetics to be able to control the material obtained by the aqueous solution route. In the present work, HA has been produced by different wet precipitation processes and different experimental conditions. Calcium hyd...

Oxygen vacancy (VO) strongly affects the properties of oxides. In this study, we used X-ray diffraction (XRD) to study changes in the VO concentration as a function of the Co-doping level of ZnO. Rietveld refinement yielded a different result from that determined via X-ray photoelectron spectroscopy (XPS), but additional maximum entropy method (MEM) analysis led it to compensate for the differe...

europium (eu) doped zno microsphere based nano-sheets were synthesized through hydrothermal method. effects of different concentrations of europium on structural and optical properties of zno nano-sheets were investigated in detail. prepared un-doped and eu-doped zno samples were characterized using x-ray diffraction (xrd), energy dispersive x-ray spectroscopy (edx), scanning electron microscop...