Neutron diffraction measurements on a single crystal of CeGe1.76 reveal a complex series of magnetic transitions at low temperature. At TN≈7 K, there is a transition from a paramagnetic state at higher temperature to an incommensurate magnetic structure characterized by a magnetic propagation vector (0 0 τ) with τ≈14 and the magnetic moment along the a axis of the orthorhombic unit cell. Below ...

Neutron diffraction data have been collected at 12, 50, 150 and 295 K for the dipeptide glycyl-L-alanine, C5H10N2O3, in order to obtain accurate positional and anisotropic displacement parameters for the H atoms. The values of these parameters serve as a benchmark for assessing the equivalent parameters obtained from a so-called Hirshfeld-atom refinement of X-ray diffraction data described else...

Triaminotrinitrobenzene (TATB) is a highly anisotropic molecular crystal used in several plastic-bonded explosive (PBX) formulations. A complete understanding of the orientation distribution of TATB particles throughout a PBX charge is required to understand spatially variable, anisotropic macroscale properties of the charge. Although texture of these materials can be measured after they have b...

Neutron scattering from protein crystals has been used successfully to determine protein structure. This technique achieves its best results when used with large crystal samples, or with samples that are amenable to techniques such as deuteration. In the case of small or delicate protein crystals, sample polarization has been identified as a method to greatly increase the signal to noise ratio ...

During investigations of phase transformation kinetics by diffraction techniques, several hundreds or even thousands of diffraction patterns are collected. Automation of the data analysis process is mandatory to perform for example a long sequence of Rietveld refinements. The Bragg edge transmission (BET) technique, a neutron time-of-flight method, allows acquiring patterns of sufficient statis...

Neutron diffraction has been used to study in situ the nanocrystallization process of Fe73.5Cu1Nb3Si22.52xBx (x55, 9, and 12! amorphous alloys. Nanocrystallization results in a decrease of both the silicon content and the grain size of the Fe~Si! phase with increasing value of x. By comparing the radial distribution function peak areas with those predicted for ideal bcc and DO3 structure, it ca...