The influence of short-time milling on the atomic structure of amorphous Co(70.3)Fe(4.7)B(25) has been investigated by differential scanning calorimetry (DSC), x-ray powder diffraction (XRD), vibrating sample magnetometer (VSM) and x-ray absorption fine-structure (XAFS) techniques. Our results prove that the milling process crystallizes the initially amorphous sample and that the degree of inhe...

Lithium ion conductors 5. Lithium Nitride Li3N 6. Lithium Lanthanum Titanium Oxide, Li3xLa0.67-xTiO3 7. Lithium Titanium Phosphate, LiTi2(PO4)3 Sodium ion conductors 8. Sodium β-Alumina, Na2O)1+x(Al2O3)11 9. Sodium β”-Alumina, Li-stabilized, Na1.5(Li0.25Al10.75)O17 10. Sodium β-Gallate, (Na2O)*n(Ga2O3) 11. Sodium β”-Gallate, Na1.98Ga10.673 O17 12. Sodium Yttrium Silicate, Na5YSi4O12 13. Sodium ...

Mesoporous aggregates of nanocrystalline zeolites with MFI and BEA frameworks have been synthesized using a one-pot and single structure directing agent. The effect of different reaction conditions, such as temperature, time, pH and water content, on the particle size, surface area and mesopore volume has been studied. Nanocrystalline and mesoporous ZSM-5, β and Y zeolites were modified with di...

The ballistic impact performance of nanocrystalline zirconia-toughened alumina (nZTA) ceramics, comprising 15 wt% nano-yttria-stabilised zirconia in a sub-micron matrix, have been studied through depth penetration tests and compared to the results for monolithic alumina. resistance each material was evaluated by fitting against thickness ceramic targets. These show that, despite micro-Raman ana...

Titanium Aluminide and TiAl matrix composites reinforced with alumina fibers (PRD166) were fabricated by powder metallurgy. During isothermal oxidation at 950 and 1070 OC, composites containing PRD166 fibers exhibited larger weight gains than monolithic TiAI; the composites showed evidence of oxidation along the perimeter of the fibers. A fiber reaction, which was observed after oxidation in ai...

the reduction of fe2o3 powder at the top layer by the volatiles from high volatile (hv) bituminous coalat the bottom layer of a multilayer powder geometry including a separating alumina layer was studied.the simultaneous effects of the alumina layer thickness, time, temperature and the weight of coal onthe amount of reduction and coal devolatilization were studied by implementing a rotatable ce...

Porous ceramic materials are of considerable interest for a variety of chemical and industrial applications in extremely harsh conditions, particularly at very high temperatures for long times. A modified gelcasting process employing agar as a natural gelling agent and polyethylene spheres as pore formers was exploited to produce porous ceramic bodies. Alumina and alumina-ZrO2 (AZ) powders were...

Abstract: Nanocrystalline MgAl2O4 spinel powder was synthesized using metal nitrates and a polymer matrix-based composed of sucrose and polyvinyl alcohol (PVA). The precursor and the calcined powders were characterized by simultaneous thermal analysis (STA), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and scanning electron microscopy (SEM). According to XRD res...