An experimental investigation of the combustion behavior of nano-aluminum (n-Al) and nano-aluminum oxide (n-Al2O3) particles stably suspended in biofuel (ethanol) as a secondary energy carrier was conducted. The heat of combustion (HoC) was studied using a modified static bomb calorimeter system. Combustion element composition and surface morphology were evaluated using a SEM/EDS system. N-Al a...

alumina is one of the most widely used ceramic materials as catalysts, catalyst supports and absorbents, and also wear resistant coating. this study focused on fabricating and characterizing of alumina ceramic nanoparticles fabricated using new and simple sol-gel method. aluminium oxide (al2o3) nanoparticles were synthesized by iron (iii) nitrate 9-hydrate as precursor. physicochemical properti...

In the present study, the gamma alumina (γ-Al2O3) nano powders have been prepared with addition of 1%mol Co using an aqueous sol-gel method at lower temperature than the pure gamma alumina. The synthesis process accomplished by partial hydrolysis of the aqueous solution of metallic ions Al3+ and Co2+, with ammonia. The Al(NO3)3.9H2O and Co(NO3)2.6H2O salts were used as cations sources. The obta...

High temperature/pressure in situ Attenuated Total Reflection Infrared (ATR-IR) spectroscopy was used to investigate the phase transformation of support γ-Al2O3 into boehmite (AlO(OH)) under the hydrothermal conditions of aqueous phase reforming (APR). Activation energy barriers of boehmite formation in hot compressed water at temperatures between 150 and 180 °C were calculated to be 15.9 ± 4.8...

The possibilities offered by catalytic γ-Al2O3 substrates are explored, and the mechanism governing graphene formation thereon is elucidated using both numerical simulations and experiments. The growth scheme offers metal-free synthesis at low temperature, grain-size customization, large-area uniformity of electrical properties, single-step preparation of graphene/dielectric structures, and rea...

Transformation of Al(NO3)3∙9H2O (upon heating in the range of 20-1200 °C) into blends of amorphous and crystalline boehmite (210-525 °C), amorphous alumina and crystalline γ-Al2O3 (850 °C), and crystalline α-Al2O3 (1100 °C) was analyzed using X-ray diffraction (XRD), high-resolution transmission electron microscope (HRTEM), infrared (IR) spectroscopy, thermogravimetry, and low-temperature nitro...

Objetivo: En este estudio se evaluó el efecto de la modificación con óxido zinc del soporte convencional en catalizadores hidrodesulfuración (HDS) a base polioxometalato Anderson-Evans NiMo5W. Metodología: Los fueron sintetizados por método co-precipitación NiMo5W sobre Al2O3. caracterizaron FRX, MEB/EDS, CHONS, propiedades texturales, FT-IR, Raman y titulación potenciométrica n-butilamina. Res...