Electron backscatter diffraction EBSD is a powerful technique applicable to a range of microstructural analyses, including texture, grain size, boundary characterization, phase distribution and inter-phase orientation relationships. The technique is suited to solving an increasing range of analytical problems on the um to mm scale. However, best results are only obtained with a good understandi...

9 Mesostructured silica phases with lamellar structure were prepared by the liquid crystal templating (LCT) technique, from double chain alkylammonium surfactant and sodium silicate or tetraethylorthosilicate (TEOS) silica precursors. The structural characterization of these phases is presented and compared. Surface modification of the silica layers, together with elimination of the organic tem...

An experimental technique has recently been developed to characterize reactive metals, including plutonium (Pu) and cerium, using electron backscatter diffraction (EBSD). Microstructural characterization of Pu and its alloys by EBSD had been previously elusive primarily because of the extreme toxicity and rapid surface oxidation rate associated with Pu metal. The experimental technique, which i...

Abstract The rheological characterization of a model, nearly ideal thixotropic carbon black suspension first proposed by Dullaert and Mewis (JNNFM 139: 21-30, 2006) is extended to include large amplitude oscillatory shear (LAOS) flow, shear flow reversal, unidirectional LAOS flow (UD-LAOS). We show how this broader data set is useful for validating and improving constitutive models of thixotrop...

Diffusion-weighted magnetic resonance spectroscopy (DWS) offers unique access to compartment-specific microstructural information on tissue, and potentially sensitive detection of compartment-specific changes in disease. The specificity of DWS is, however, offset by its relative low sensitivity, intrinsic to all MRS-based methods, and further exacerbated by the signal loss due to the diffusion ...

Glassy carbon (GC) is an amorphous yet sp rich allotrope of carbon that has received a lot of attention as an electrode material in Li ion batteries. In this contribution we explore the microstructural, thermal and mechanical properties of GC derived from the pyrolysis of lithographically patterned SU8, which is the most common precursor polymer in CMEMS (carbon microelectromechanical systems)....

Electron backscatter diffraction (EBSD) has evolved into a well-established tool for microstructural characterization by providing quantitative information on crystallographic orientation and phase content and distribution. The rapid acceptance of EBSD as an analytical technique has been driven, in part, by the highly informative contrasts used to create different micrographs which effectively ...

Two limestones are studied to compare the fragmentation pattern induced by dynamic loads. A quasi-static characterization allows one to determine the basic mechanical properties and to compare the two rocks in terms of Weibull parameters, indicators of microstructural differences. Edge-on impacts are performed and show the important role of the Weibull modulus in the fragmentation pattern. Simu...

Synchrotron Radiation Facilities, supported by the Materials Science and Engineering Laboratory of the National Institute of Standards and Technology, include beam stations at the National Synchrotron Light Source at Brookhaven National Laboratory and at the Advanced Photon Source at Argonne National Laboratory. The emphasis is on materials characterization at the microstructural and at the ato...

The aim of this work is to develop a new hyperelastic and anisotropic material mimicking histological and mechanical features of healthy and aneurysmal arterial tissues. The target material is constituted by rhombic periodic lattices of hyperelastic fibres embedded into a soft elastomer membrane. Based on a previous theoretical work yielding to an optimized microstructural arrangement and mecha...