The aim of our study was to investigate the amount of 110 pesticide residues in cereals and foodstuff from Poland as a part of official control. A total of 89 samples were collected in 2009-10. In 84.2% of the samples no residues were found: 15.8% of samples contained pesticide residues below the maximum residue limit. Pirimiphos-methyl was the most frequently found pesticide. The results show ...

background: pistachio is one of the main nutrients, not only as a strategic crop but also as a main type of nut, in iranians’ food cycle. the aim of this study was to measure the relative safety of iranian pistachio based on the standard pesticide’s residue limits, which should be monitored and assessed in the cultivation of pistachio in order to confirm its public health. methods: fifty sample...

This work presents the development of bioassays and biosensors for the detection of insecticides widely used in the treatment of olive trees. The systems are based on the covalent immobilisation of acetylcholinesterase on magnetic microbeads using either colorimetry or amperometry as detection technique. The magnetic beads were immobilised on screen-printed electrodes or microtitration plates a...

In accordance with the maximum residue limit of 100 micrograms kg-1 established by EU legislation, a simple and sensitive high-performance liquid chromatographic (HPLC) method was developed for the measurement of tylosin residues in pig tissues (fat, kidney, liver and muscle). Tylosin, a macrolide antibiotic, is extracted with water-methanol and cleaned-up by solid-phase extraction (SPE) on cat...

Milk samples from 28 cows were analysed for residues of oxacillin after drying off with Stapenor Retard TS (oxacillin). Analysis was performed with an automated HPLC system consisting of an on-line solid-phase extraction and photochemical post-column derivatization with UV-detection at 300 nm. Although the time interval between treatment and parturition was less than the demanded 55 days, the m...

Interfering maximum residue limits (MRLs) for pesticides with agricultural trade is becoming important food and policies in the early 21st century. Differing levels pesticide residues among countries have potential to disrupt significantly. We employ a non-linear disaggregated stringency index quantify degree of regulatory heterogeneity between trading nations fruits vegetables 2013 2014 invest...