nanocrystalline zinc oxide (zno) powders with different morphology have been successfully synthesized by using different surfactants such as cetyl trimethyl ammonium bromide (ctab), sodium dodecyl sulphate (sds), and tri ethanol amine (tea) via hydrothermal method. the products were characterized by means of powder x-ray diffraction (xrd), scanning electron microscopy (sem), transmission electr...

in this investigation, hydroxyapatite (hap) nanostructure with uniform morphologies, controllable size, nano-dispersion and narrow-size distribution in diameter has been synthesized successfully by low-temperature hydrothermal process, and the as-synthesized powders were characterized by energy-dispersive x-ray spectroscopy, scanning electron microscopy, high-resolution transmission electron mi...

In the present work, we report a suitable approach for the preparation of BaTiO3 nanostructures via the hydrothermal condition using Dolapix ET85 as surfactant. The powders were investigated by X-ray diffraction (XRD), scanning election microscopy (SEM), energy-dispersive X-ray spectroscopy (EDAX), field emission transmission electron microscopy (FETEM), selected area electron diffra...

Cu/Cu2O nano-heterostructure hollow spheres with a submicron diameter (200-500 nm) were prepared by a microwave-assisted hydrothermal method using Cu(OAc)2·H2O, PVP and ascorbic acid solution as the precursors. The morphology of the products could evolve with the hydrothermal time from solid spheres to thick-shell hollow spheres, then to thin-shell hollow spheres, and finally to nanoparticles. ...

In this study, hydroxyapatite (denoted as HAp) nanostructure with uniform morphologies, controllable size, nano-dispersion and narrow size distribution in diameter has been synthesized successfully by low-temperature hydrothermal process, and the as-synthesized powders were characterized by XRD, scanning electron microscopy, high-resolution transmission microscopy, FT-IR, Zetasizer and inductiv...

Starting from Ni-Co-Mn carbonate nanoparticles prepared by microreaction technology, uniform spherical particles of Ni1/3Co1/3Mn1/3CO3 with a size of 3–4 μm were obtained by a controllable hydrothermal conversion with the addition of (NH4)2CO3. Based on characterizations on the evolution of morphology and composition with hydrothermal treatment time, we clarified the mechanism of this novel met...

In this paper, we focus on the controlled growth mechanism of α-Fe2O3 nanostructures via the hydrothermal method. The field emission scanning electron microscopy (FESEM) results reveal that at a lower hydrothermal time, the initial nucleation involves the formation of short and thin β-FeOOH nanorods. The subsequent increase in the hydrothermal time leads β-FeOOH to form thicker and longer nanor...

Cobalt ferrite nano-powder have been obtained through a hydrothermal method with 2:1 molar ratio of Fe:Co without using any surfactant. X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM) were used to consider the structural and morphological properties of CoFe2O4 nano-particles. Also, EDAX spectroscopy applied to evaluate the chemical composition. Results demonstrated that 15 hr hyd...