نتایج جستجو برای: heating up solution synthesis

تعداد نتایج: 1769533  

2012
Kadir Ozden Yerdelen

In this study, solvent-free and phase transfer catalysis conditions coupled with microwave irradiation and their advantages in synthesis of N-alkylation of primary anilines were reported. In this way two different microwave processing techniques were compared in terms of reaction yields. Consequently, microwave irradiation significantly reduced reaction times compared to traditional heating met...

2016
Sotirios A. Kyriakis Paul L. Younger

Geothermal energy is a renewable energy source which can provide base-load power supply both for electricity and direct uses, such as space heating. In this paper, district heating systems that are fed by geothermal energy, the so-called geothermal district heating systems, are studied. It is proposed to apply a hot water storage tank in these systems to store hot water in times of low-load and...

2009
Koichi SHIBUYA Shoji KAWASAKI Masahiro KURODA Jun-ichi ASAUMI Koichi Shibuya

Thermotolerance in tsAF8 cells develops during incubation at 34°C after heating at 4SoC, while it is suppressed by the following incubation at a non-permissive temperature of 39.7"C after the same heating. The incubation temperature after heating may affect the cell cycle and consequently thermotolerance. In the present study, a relationship between the thermotolerance and the cell cycle of tsA...

2010
Michael J. Holst Mats G. Larson Axel Målqvist Robert Söderlund

In this paper we present a finite element discretization of the Joule-heating problem. We prove existence of solution to the discrete formulation and strong convergence of the finite element solution to the weak solution, up to a sub-sequence. We also present numerical examples in three spatial dimensions. The first example demonstrates the convergence of the method in the second example we con...

Journal: :Dalton transactions 2015
Marco Taddei Phuong V Dau Seth M Cohen Marco Ranocchiari Jeroen A van Bokhoven Ferdinando Costantino Stefano Sabatini Riccardo Vivani

A highly efficient and scalable microwave assisted synthesis of zirconium-based metal-organic framework UiO-66 was developed. In order to identify the best conditions for optimizing the process, a wide range of parameters was investigated. The efficiency of the process was evaluated with the aid of four quantitative indicators. The properties of the materials prepared by microwave irradiation w...

2015
Junzhi Yang Paul R. Beaumont Terry D. Humphries Craig M. Jensen Xingguo Li Enrico Sciubba

A novel species of metal amidoborane ammoniate, [Al(NH2BH3)63−][Al(NH3)63+] has been successfully synthesized in up to 95% via the one-step reaction of AlH3·OEt2 with liquid NH3BH3·nNH3 (n = 1~6) at 0 °C. This solution based reaction method provides an alternative pathway to the traditional mechano-chemical ball milling methods, avoiding possible decomposition. MAS 27Al NMR spectroscopy confirm...

2018
Adrien Le Coënt Laurent Fribourg Nicolas Markey Florian De Vuyst Ludovic Chamoin

We present a correct-by-design method of state-dependent control synthesis for sampled switching systems. Given a target region R of the state space, our method builds a capture set S and a control that steers any element of S intoR. The method works by iterated backward reachability fromR. The method is also used to synthesize a recurrence control that makes any state of R return to R infinite...

Journal: :Acta Metallurgica Slovaca 2021

Transparent MgAl2O4 ceramics were fabricated by pulsed electric current sintering (PECS) employing two-step mode. First, nanoscale powders produced solution combustion synthesis from hydrated nitrate compounds and urea. Subsequently, the synthesized sintered PECS with a heating rate of 100oC/min under an applied pressure 100 MPa. The process was conducted according to profile. At first step, te...

Journal: :Journal of virology 1970
M Margalith E Margalith T Nasialski N Goldblum

Heating to 45 C induced in virus-free clones of simian virus 40 (SV40) transformed BSC(1) cells the synthesis of SV40 viral antigen, as evidenced by immunofluorescence. Up to 3.8% of the cells exhibited viral antigen 72 hr after heating to 45 C for 30 min. Depletion of arginine from the medium of the heated cells enhanced and increased the percentage of cells synthesizing viral antigen to 11%. ...

Journal: :Nanoscale 2013
Xin Liu Mark T Swihart

Here we demonstrate a single-pot heating approach for controllable synthesis of colloidal zinc oxide nanocrystals from zinc acetylacetonate. Such single-pot heating approaches are inherently amenable to large scale production. We have systematically studied the crystallization process, investigating the growth of nanocrystals and the influence of ligands on the morphology and luminescence of Zn...

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