in this study, an attempt has been made to study the effect of bi2o3 addition as nucleating agent on the liquid-liquid phase separation, crystallization and dielectric properties of samples prepared by sintering and crystallization of powdered glass in pbo-tio2-b2o3-sio2 glass-ceramic system using dta, xrd, sem and lcr techniques. the results showed that the addition of bi2o3 resulted in a quit...

Two glass ceramics in the CaO--P2O5--MgO system with the incorporation of K2O or TiO2 oxides were prepared with the goal of using them as potential bone graft substitutes. The incorporation of TiO2 and K2O led to the preparation of specific crystalline phases in the structure of the glass ceramics, which show different degrees of biodegradation. In fact, the 45CaO--45P2O5--5MgO--5K2O has been p...

introduction: the purpose of the presented study was to evaluate the effect of zirconia thickness on the tensile stress of zirconia based all-ceramic restorations. methods: twenty zirconia disks with 10mm diameter were prepared in two groups using cad/cam system. the thickness of zirconia was 0.5mm in first group and 0.3mm in second group. after sintering, 0.4mm glass ceramic porcelain was appl...

A conducting lithium aluminum germanium phosphate (LAGP) glass-ceramic with a formula of Li1.5Al0.5Ge1.5(PO4)3 was synthesized by melt-quenching method and subsequent crystallization at 850 °C for 8 h. The prepared glass-ceramic was characterized using differential scanning calorimetry (DSC), X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), and AC impedance techniqu...

The effect of iron oxide content on the crystallisation of a diopside glass–ceramic glaze was investigated using a glass–ceramic frit in the K2O–ZnO–MgO–CaO–Al2O3–SiO2 system and a granite waste glass. Measurements by X-ray diffraction (XRD) combined with scanning electron microscopy (SEM) and EDX microanalysis showed that the distribution of Fe ions among different crystalline phases such as f...

The bioactive glass 45S5 was crystallized to 8-100 vol % of crystals by thermal treatments from 550-680 degrees C. The micro-structure of the glass-ceramics had a very uniform crystal size, ranging from 8 to 20 microns. Fourier-transform infrared (FTIR) spectroscopy was used to determine the rate of hydroxycarbonate apatite (HCA) formation that occurs on bioactive glass and glass-ceramic implan...

The present study aimed to evaluate the influence of various heat-pressing procedures (different holding time and heat pressing temperature) on the microstructure and flexural strength of lithium disilicate glass ceramic. An experimental lithium silicate glass ceramic (ELDC) was prepared from the SiO2-Li2O-K2O-Al2O3-ZrO2-P2O5 system and heat-pressed following different procedures by varying tem...

The development of bioactive glass-ceramic materials has been a topic of great interest aiming at enhancing the mechanical strength of traditional bioactive scaffolds. In the present study, we test and demonstrate the use of Biosilicate® glass-ceramic powder to fabricate bone scaffolds by the foam replica method. Scaffolds possessing the main requirements for use in bone tissue engineering (95%...

Waste derived glass ceramic composites prepared by low temperature sintering/sinter-crystallisation I. Ponsot, R. Detsch, A. R. Boccaccini & E. Bernardo To cite this article: I. Ponsot, R. Detsch, A. R. Boccaccini & E. Bernardo (2015) Waste derived glass ceramic composites prepared by low temperature sintering/sinter-crystallisation, Advances in Applied Ceramics, 114:sup1, S17-S25, DOI: 10.1179...