A method for the analysis of several volatiles compounds responsible for orange juice flavour (ethyl butanoate, limonene, linalool, alpha-pinene, geranial, neral and alpha-terpineol) has been developed. The isolation of this compounds was carried out by pervaporation (PV) followed by on-line gas chromatography-mass spectrometry (GC-MS). The coupling PV-GC-MS has been successfully applied to fre...

in this study, aerial parts of lippia citriodora kunth were harvested at three phenological stages (i.e. vegetative, full flowering and fruit set). the essential oil isolated by hydro distillation for 3 h using a clevenger-type apparatus and the oil was analyzed by gc and gc-ms. the yields of oils (w/w%) in different stages was in the order of: full flowering (0.9%), vegetative (0.48%) and frui...

The volatile constituents of the aerial parts of vervain (Verbena officinalis L.) cultivated locally were investigated. Analysis of the volatile fraction by GC and GC-MS is described. Compounds were identified by various methods, the major compounds being 3-hexen-1-ol (7.28%), 1-octen-3-ol (32.76%), linalool (4.66%), verbenone (20.49%) and geranial (7.22%).

Traditional hydrodistillation (HD), steam distillation extraction (SD), organic solvent extraction (SE), and microwave assisted hydrodistillation (MWHD) techniques were compared and evaluated for their effectiveness in the isolation of essential oil of Melissa officinalis from Algeria. The microwave assisted hydrodistillation technique was optimized in terms of both delivered power and time dur...

Trypanocidal activity was found in the volatile oil of dried Dracocephalum kotschyi. GC-MS analysis determined that the major constituents of the oil were geranial (35.8%), C10H14O (26.6%), limonene (15.8%) and 1,1-dimethoxy decane (14.5%). In order to isolate the unknown biologically active monoterpene, fractionation of the volatile oil was carried out by silica gel column chromatography. The ...