OBJECTIVE This study was conducted to determine molecular structures related to carbohydrates and lipid in alfalfa hay cut at early bud, late bud and early flower and in the afternoon and next morning using Fourier transform infrared spectroscopy (FT/IR) and to determine their relationship with alfalfa hay nutrient profile and availability in ruminants. METHODS Chemical composition analysis, ...

Multi-walled carbon nanotubes (MWCNTs) were functionalized using nonequilibrium atmospheric pressure plasma. The efficiency of the atmospheric pressure plasma treatment is characterised by XPS, FT-IR spectroscopy and contact angle measurements. Scanning electron microscopy (SEM) reveals that the MWCNT structure can be preserved when wet feeding into the plasma is applied.

FT-IR spectroscopy is the basic finger-print method for qualitative and quantitative analysis of nitrogen, boron, hydrogen impurities in natural synthetic diamonds. In measurements impurity concentrations, external standard samples are required calibration procedure during analysis. this study, double-phonon mid-IR absorption coefficient optical phonons diamond host matrix, robust internal stan...

Hybrid microspheres of calcium carbonate/fullerenol were synthesized and characterized. Their morphology depends on the concentration of the fullerenol solutions. XRD and FT-IR measurements proved that the mineral phase is consistently calcite, while fluorescence confocal microscopy indicated that fullerenol is homogenously included in the crystalline matrix.

In this research, Novel UV curable conductive nanocomposites containing urethane acrylate and PANi-Co3O4 nanocomposite have been prepared. At first, PANi- Co3O4 nanocomposites have been synthesized and then PUA-PANi-Co3O4 nanocomposites films were prepared by ultraviolet radiation. UV-Vis and FT-IR studies confirm that there was strong chemical interaction between PANi and Co3O4 nanoparticles, ...

Photo-oxidative stability of a series of most common red acrylic paints has been investigated. The paints in question were carmine, quinacridone scarlet, alizarin crimson, brilliant red, vermilion and cadmium red hue. Structural changes, discoloration and weight loss of paints film subjected to UV irradiation in an accelerated ageing chamber were measured using FT-IR spectroscopy, colorimetry a...

BACKGROUND Kidney stones are a common illness with multifactorial etiopathogenesis. The determination of crystalline and molecular composition and the quantification of all stone components are important to establish the etiology of stones disease but it is often laborious to obtain using the chemical method. The aim of this paper is to compare chemical spot test with FT-IR spectroscopy, for a ...

An evaluation of high-throughput Fourier-transform infrared spectroscopy (FT-IR) as a technology that could support a "metabonomics" component in toxicological studies of drug candidates is presented. The hypothesis tested in this study was that FT-IR had sufficient resolving power to discriminate between urine collected from control rat populations and rats subjected to treatment with a potent...

The present work describes the synthesis and characterization of a few Mn(III) porphyrins with imidazole. A new series of high-spin Mn(III) porphyrins having general formulae [Mn(THMPP)X] and [Mn(THMPP)X(Im)], where THMPP = Tetrakis(4-hydroxy-3-methoxyphenyl) porphinato ligand, X = Cl − , Br − , N3 or NCS − and Im = Imidazole have been synthesized. These complexes have been characterized by UV...

Terahertz time-domain spectroscopy (THz-TDS) and Fourier transform infrared (FT-IR) spectroscopy were used to generate far-infrared and low-frequency spectral measurements of monomeric lysozyme and lysozyme fibrils. The formation of lysozyme fibrils was verified by the Thioflavin T assay and transmission electron microscopy (TEM). It was evident in the FT-IR spectra that between 150 and 350 cm(...