We demonstrate Zernike phase contrast in a compact soft x-ray microscope using a single-element optic. The optic is a combined imaging zone plate and a Zernike phase plate and does not require any additional alignment or components. Contrast is increased and inversed in an image of a test object using the Zernike zone plate. This type of optic may be implemented into any existing x-ray microsco...

In this contribution we present source properties and design considerations for a compact x-ray microscope operating in the water-window spectral region at 2.48 nm. The microscope will use a liquid-nitrogen-jet laser-plasma source with sufficient brightness, uniformity, stability and reliability for microscopy operation. The source is quantitatively characterized by calibrated slitgrating spect...

We demonstrate high-resolution x-ray differential interference contrast DIC in a compact soft x-ray microscope. Phase contrast imaging is enabled by the use of a diffractive optical element objective which is matched to the coherence conditions in the microscope setup. The performance of the diffractive optical element objective is evaluated in comparison with a normal zone plate by imaging of ...

X-ray crystallographic methods and electron microscope image analysis have been used to correlate the structure and the chemical composition of gap junction plaques isolated intact from mouse liver. The requirement that the interpretations of X-ray, electron microscope, and chemical measurements be consistent reduces the uncertainties inherent in the separate observations and leads to a unified...

in the present work, bi2s3 nanostructures have been synthesized with the aid of thioglycollic acid (tga) a solvent, capping agent, and sulfide source in the presence of ultrasonic method. the as-synthesized products were characterized by x-ray diffraction (xrd), energy dispersive x-ray spectroscopy (eds), scanning electron microscope (sem), and photoluminescence (pl) spectroscopy. the band gap ...

oxide nanoparticles of fe-co-ni were prepared in six different compositions by co-precipitation method. the as-synthesized nanoparticles were characterized by x-ray diffraction (xrd), field emission scanning electron microscope (fesem), fourier transform infrared (ft-ir) and vibrating sample magnetometer  (vsm). it was found that the nanoparticles had mean crystalline size of 30-55 nm and spher...

ZnO nanostructure films were deposited by radio frequency (RF) magnetron sputtering on etched silicon (100) substrates using dry Ar/SF6 plasma, at two etching times of 5 min and 30 min, and on non etched silicon surface. Energy dispersive X-ray (EDX) technique was employed to investigate the elements contents for etched substrates as well as ZnO films, where it is found to be stoichiometric. Su...

Nickel films of 300 nm thickness were deposited by electron beam evaporation at room temperature on 316 stainless steels. Corrosion studies of Ni coated 316 SS have been performed after N+ ion implantation at different energies of 20, 40, 60 and 80 keV. The structure and surface morphology of the films were evaluated using X-ray diffraction (XRD), atomic force microscope (AFM) an...