oxide nanoparticles of fe-co-ni were prepared in six different compositions by co-precipitation method. the as-synthesized nanoparticles were characterized by x-ray diffraction (xrd), field emission scanning electron microscope (fesem), fourier transform infrared (ft-ir) and vibrating sample magnetometer  (vsm). it was found that the nanoparticles had mean crystalline size of 30-55 nm and spher...

in the present work, we report a suitable approach for the preparation of batio3 nanostructures via the hydrothermal condition using dolapix et85 as surfactant. the powders were investigated by x-ray diffraction (xrd), scanning election microscopy (sem), energy-dispersive x-ray spectroscopy (edax), field emission transmission electron microscopy (fetem), selected area electron diffraction (saed...

Tellurium nanostructures have been prepared by physical vapor deposition method in a tube furnace. The experiments were carried out under argon gas flow at a pressure of 1 mbar. Tellurium powder was evaporated by heating at 350°C and 430°C and was condensed on substrates at 110–250°C, in the downstream of argon gas flow. The products were characterized by field emission scanning electron micros...

Tellurium nanostructures have been prepared by physical vapor deposition method in a tube furnace. The experiments were carried out under argon gas flow at a pressure of 1 mbar. Tellurium powder was evaporated by heating at 350°C and 430°C and was condensed on substrates at 110–250°C, in the downstream of argon gas flow. The products were characterized by field emission scanning electron micros...

Recently, Prussian blue analogues (PBAs) have been reported to exhibit a low voltage charge/discharge behavior with high capacity (300–545 mAh/g) in lithium-ion secondary batteries (LIBs). To clarify the mechanism of low voltage behavior, we performed ex situ synchrotron radiation X-ray diffraction (XRD) and ex situ X-ray absorption spectroscopy (XAS) of a film of Na1.34Mn[Fe(CN)6]0.84·3.4H2O w...

Magnesium oxide nanoparticles were synthesized using Arabic gum as a biotemplate andmagnesium nitrate as the magnesium source by the sol-gel method. This method has manyadvantages such as nontoxic, economic viability, ease to scale up, less time consuming andenvironmental friendly approach for the synthesis of MgO nanoparticles without using anyorganic chemicals. Nanoparticles were characterize...

The use of plant extract is generating the interest of researchers toward cost effective,nontoxic, economic viability and eco-friendly green synthesis of nanoparticles. In the presentwork, zinc oxide (ZnO) nanoparticles were synthesized using black tea extract and zinc nitrateas the zinc source by the sol-gel method. The synthesized ZnO nanoparticles werecharacterized by powder X-ray diffractio...

A filter based on the Hankel Lanczos Singular Value Decomposition (HLSVD) technique is presented and applied for the first time to X-ray diffraction (XRD) data. Synthetic and real powder XRD intensity profiles of nanocrystals are used to study the filter performances with different noise levels. Results show the robustness of the HLSVD filter and its capability to extract easily and efficiently...

X-ray diffraction (XRD) and electron backscatter diffraction (EBSD) are commonly used to perform texture analysis of thin films. However, due to principle differences in data acquisition these techniques can yield disagreeing results. In this paper, we aim to highlight possible error sources with given examples for aluminum and copper thin films. INTRODUCTION Texture in materials has a large in...

Nano size nickel copper ferrite powders (NiCuFe2O4) have been prepared by a prepared by Co precipitation method. The resulting powders were characterized by X-ray diffraction (XRD), Scanning electron microscope (SEM).The result showed nanosize nickel copper ferrite(35.65nm). The powders showed extensive XRD line broadening and sizes of crystals observed from the XRD line broadening was35.65 nm,...