نتایج جستجو برای: water as solvent
تعداد نتایج: 5981458 فیلتر نتایج به سال:
Hexane, the common solvent for extraction of edible oils from seeds is no more considered safe due to the presence of solvent in oil and also solvent vapour, a hazardous air pollutant. We have carried out the experiments with bahera (Terminalia bellerica Roxb) and flax seed (Linum usitatissimum ) oil as these oils are highly used in food for their nutraceutical values. The extraction of edible ...
The impact of extraction methodology and polarity of extraction solvents on the assay of phenolic compounds was investigated using parsley (Petroselinum crispum) flakes as a model substrate. This systematic study was undertaken to address substantial variations in the extraction procedures, solvents and conditions as described in the recent literature. Five different extraction procedures [shak...
هدف اصلی این رساله ارائه روش های نوین سنتزی در راستای اهداف شیمی سبز می باشد. استفاده از روش های سنتزی مانند انجام واکنش در محیط های مایی، واکنش های بدون حلال و استفاده از کاتالیزگرهای آلی مبنای انجام واکنش ها در طرح حاضر بوده است. بر این اساس تحقیقات انجام شده در این پایان نامه به چهار بخش تقسیم شده است که در ادامه خلاصه ای از هر یک از فصول توضیح داده خواهد شد: در بخش 1، روشی جدید برای تهیه ف...
the dispersive liquid–liquid microextraction (dllme) method for determination of pb +2 and cd +2 ions in the environmental water samples was combined with inductively coupled plasma-atomic emission spectrometry (icp-aes). ammonium pyrrolidine dithiocarbamate (apdc), chloroform and ethanol were used as chelating agent, extraction solvent and disperser solvent, respectively. some effective parame...
Atomistic simulations are used to characterize the molecular dynamics (MD) of alkyl chains with different functionalizations in different water/acetonitrile mixtures (80/20 and 50/50). Starting from fully equilibrated solvent systems (flat density profile for both components), microheterogeneous structuring of the solvent in the chromatographic system is found for both mixtures. Depending on th...
Ultrasonic & Viscometric studies of glycine and other amino acids have been carried out in methanol + water and propanol-1 + water co-solvents at different temperatures 30, 35 and 40°C respectively. Various thermodynamic parameters such as apparent molal compressibility and their limiting values have been determined. The results are discussed in the terms of solute – solvent interactions in alc...
Focused open-vessel microwave-assisted extraction (FOV-MAE), closed-vessel microwave-assisted extraction (CV-MAE), and accelerated solvent extraction (ASE) were used for extraction before determination of organochlorine compounds (polychlorinated biphenyls, DDT, toxaphene, chlordane, hexachlorobenzene, hexachlorocyclohexanes, and dieldrin) in cod liver and fish fillets. Wet samples were extract...
Cellular metabolome analysis by chromatography-mass spectrometry (MS) requires prior metabolite extraction. We examined a diversity of solvent systems for extraction of water-soluble metabolites from Escherichia coli. Quantitative yields of approximately 100 different metabolites were measured by liquid chromatography-tandem MS and displayed in clustered heat map format. Many metabolites, inclu...
Integral equation theory is used for extrapolating free energy data from molecular simulations of a reference state with respect to a modification of the interaction potential. The methodology is applied to the correction of artefacts arising from potential shifting and truncation. Corrective contributions for the hydration free energy with respect to the full potential are analysed for the cas...
The condensation of benzylamine with glyoxal leads to Hexabenzylhexaazaisowurtzitane (HBIW) in acetonitrile solvent with citric acid as a green catalyst under both conventional stirring and ultrasonic irradiation conditions. The influence of four variables, including the amount of catalyst, solvent, reaction time and ultrasonic power, on the reaction yield was investigated. The results showed t...
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