With the aim to enhance interfacial adhesion of a hydrophobic polymer matrix and cellulosic fibers and fillers, chemical surface modifications with silane coupling agents are performed. Thermogravimetric analysis (TGA) could be used to determine the degree of surface functionalization. However, similar thermal properties of treated and untreated cellulose hamper a precise determination of silan...

The authors have studied the effect of plasma power, reactor outgassing rates, and of silane purity on the oxygen, carbon, and nitrogen contents of amorphous silicon material prepared by the very high frequency ~70 MHz! glow discharge technique. The silane purity could be optionally enhanced by the application of a getter-based silane gas purifier. It was found that oxygen incorporation was enh...

This study assessed the effect of different etching time of hydrofluoric acid and ultrasonic cleaning of the etched ceramic surface on the resin microtensile bond strength stability to a feldspathic ceramic. The research hypotheses investigated were: (1) different etching time does not affect the adhesion resistance; (2) ultrasonic cleaning improves the adhesion resistance. Forty-eight (48) blo...

BACKGROUND AND OBJECTIVES Acrylic resin ruled the dental profession for 60 years, and this success is attributed to its aesthetics, handling properties, physical and biological compatibility, its stability in oral environment and its cost effectiveness. The objective of this study is to evaluate and compare the bond strength of acrylic resin teeth treated with various conditioning materials lik...

The objective of this study was to investigate the rebonding effect of a new silane coupling agent on various ceramic brackets bonded to ceramic specimen. Different ceramic brackets (Fascination 2, Clarity SL, and In-OvationC) were assigned to three groups: rebonding with new silane coupling agent, rebonding with conventional silane coupling agent, or regular bonding as control (n = 16). Bracke...

Two grades of metallocene-catalysed LLDPE and one grade of low-density polyethylene (LDPE) have been silane grafted and crosslinked by contact with water and their performance has been compared and evaluated. The effects of vinytrimethoxysilane (VTMOS) levels on the degree of crosslinking for each grade were also studied. It was found that increasing level of silane increases the degree of cros...

OBJECTIVE To assess four different chemical surface conditioning methods for ceramic material before bracket bonding, and their impact on shear bond strength and surface integrity at debonding. METHODS Four experimental groups (n = 13) were set up according to the ceramic conditioning method: G1 = 37% phosphoric acid etching followed by silane application; G2 = 37% liquid phosphoric acid etch...

OBJECTIVES The aim of this study was to evaluate the effect of different surface treatments on the microtensile bond strength between a leucite reinforced glass-ceramic and composite resin. METHODS Leucite reinforced ceramic blocks (n=24) were constructed using the hot pressing technique. The blocks were assigned to 4 groups, which received the following surface treatments: G1: hydrofluoric (...

The aim of this study was to compare the effects of various porcelain surface-conditioning techniques, used either alone or in combination, on the shear bond strength (SBS) of ceramic brackets cured with a light emitting diode (LED). Thirty glazed porcelain facets were randomly divided into three groups of 10. In group I, the porcelain surfaces were etched with 9.6 per cent hydrofluoric acid (H...

Natural fiber as reinforcement filler in polymer composites is an attractive approach due to being fully biodegradable and cheap. However, incompatibility between hydrophilic natural fiber and hydrophobic polymer matrix restricts the application. The current studies focus on the effects of incorporation of silane treated OPMF into polylactic acid (PLA)/polycaprolactone (PCL)/nanoclay/OPMF hybri...