A capillary electrophoresis method has been established for the determination of triptonide and triptolide in Multi-glycosides Tripterygium wilfordii tablets. Capillary separation was carried out by using 0.01mol L borax + 0.02 mol L boric acid + 0.02 mol L SDS (pH = 8.0) as the buffer, a fused – silica capillary tube column (60.2 cm × 75μm id. 52.6 cm of effective length) as the separation cha...

Capillary porosity percolation in a hydrating cement paste has a large influence on transport properties and durability. Percolation can be examined using low-temperature calorimetry and using microstructure models. In this paper, the two approaches are compared for cement pastes with different water-to-cement ratios and exposed to various curing conditions. The influence of sealed curing is se...

Thermal transpiration is a rarefied gas flow driven by a wall temperature gradient and is a promising mechanism for gas pumping without moving parts, known as the Knudsen pump. Obtaining temperature measurements along capillary walls in a Knudsen pump is difficult due to extremely small length scales. Meanwhile, simplified analytical models are not applicable under the practical operating condi...

Abstract Capillary heat exchangers are a great alternative to conventional radiators or electric heaters when used with pumps due larger area and therefore lower working temperature. In this work, we study thermal conditions in model room using either capillary heaters. Experimental measurements special test building validate adjust numerical models. The results show that the vertical temperatu...

A capillary tube is widely used as an expansion device for small refrigeration cycles. Recently, immiscible oil is sometimes used in the refrigeration cycle to improve severe lubricating conditions and to prevent blockage of the capillary tube caused by the hydrolysis of ester oil. This paper discusses the influence of mixing of the immiscible oil with the refrigerant on the flow characteristic...

a) Run the program HPCESIM. Copy all basic parameters (Equipment, Capillary, Buffer, Sample, Inject and Detect) for electrophoretic separation of mixture of 4 organic acids into table 1. Table 1 Voltage U (kV) Current I (μA) Thermostating temperature T (oC) Capillary length to detector L (mm) ID (inner diameter of capillary) (μm) Separation mode (anionic/cationic) Composition of basic electroly...

A range of complex percutaneous procedures, such as biopsy or regional anesthesia, rely heavily on accurate needle insertion. Small variations in the mechanical properties of the pierced tissue can however cause deviations from the projected needle path and can thus result in inaccurate placement of the needle. Navigation of a rigid needle towards the target tissue is traditionally based on the...

the reaction of ch3o2 radicals with acetaldehyde on the solid surface of nh4no3 has been studied in a flow capillary reactor at low pressure and room temperature. the experiments were performed using epr spectrometer combined with the kinetic method of radicals freezing. peroxy radicals revealed an oscillation complex behavior during the process regarding to the phenomenon of radicals multiplic...

DNA sequencing by capillary electrophoresis has been reviewed with an emphasis on progress during the last four years. The effects of sample purification, composition of sieving matrices, electric field strength, temperature, wall coating and DNA labeling on the DNA sequencing performance are discussed. Multicapillary array instrumentation is compared with one-capillary systems. Integrated syst...

This work presents a novel method for the accurate determining trans- and cis-resveratrol (3,5,4'-trihydroxystilbene) by nonaqueous capillary electrophoresis/fluorescence spectroscopy at 77 K. The proposed method permits not only the separation of resveratrol isomers, but also ensures that on-line spectra are readily distinguishable and unambiguously assigned. The experimental results also indi...