نتایج جستجو برای: synthesis condition

تعداد نتایج: 718543  

A Highly efficient protocol has been developed for the synthesis of 2-hydrazolyl-4-thiazolidinone derivatives installing a one pot three component coupling reaction of an aromatic aldehyde, thiosemicarbazide and maleic anhydride using guanidine hydrochloride as highly inexpensive and environmentally friendly catalyst under solvent free condition at 1200C with good to excellent yields, It offers...

Journal: :iranian journal of catalysis 2015
leila dinparast hassan valizadeh

freshly prepared zno nanoparticles were used as an effective heterogeneous base catalyst for the synthesis of aryloximes. the conversion of arylaldehydes and arylketones into the corresponding oximes (up to quantitative yields) was achieved by simply mixing the liquid reactants and hydroxylamine hydrochloride with zno nanoparticles under solvent-free condition. the procedure was carried out und...

2015
Fan Long Zichao Qi Sara Achour Martin Rinard

We present PCR, a new automatic patch generation system. PCR uses a new condition synthesis technique to efficiently discover logical expressions that generate desired controlflow transfer patterns. Presented with a set of test cases, PCR deploys condition synthesis to find and repair incorrect if conditions that cause the application to produce the wrong result for one or more of the test case...

2001
Jun Ji

In this paper I compared imaging conditions of three different prestack migrations in terms of angle-dependent reflectivity recovery. The imaging conditions compared are shot profile migration with conventional imaging condition, de Brduin’s imaging condition, and planewave synthesis imaging. The conventional imaging condition can be applied to any reflector geometry and to arbitrary velocity, ...

2009
Ling Cen Minghui Dong Paul Y. Chan Haizhou Li

Synthesized speech can be largely degraded in noise, resulting in compromised speech quality. In this paper, we propose a unit selection based speech synthesis system for better speech quality under poor channel conditions. First, the measurement of speech intelligibility is incorporated in the cost function as a searching criterion for unit selection. Next, the prosody of the selected units is...

2010
Esther-Sabrina Wacker Joachim Denzler

A regular rope quality inspection is compulsory for wire ropes in security-relevant applications. Principal procedures of such quality checks are the visual inspection for surface defect detection, the magnetic inspection for a localization of broken wires and the measurement of the rope diameter. However, until today it is hardly possible for the human inspector to measure other important rope...

An efficient, simple and convenient route is described for the synthesis of biscoumarin (3,3'-(arylmethylene) bis (4-hydroxy-2H-chromen-2-one)) by using of recyclable catalyst TiO2@KSF. In this Method, we synthesis biscoumarin derivatives via 3multi-component reactions (3MCRs) of two equivalent 4-hydroxycoumarin with one equivalent of aromatic aldehydes using 20 mg nano TiO2@KSF as homogeneous ...

One of the important Multi-component reaction (MCRs) is the synthesis of dihydropyrano chromene derivatives by one-pot reaction. In this research, an inexpensive and effective one pot three component procedure with good yields for the synthesis of dihydro pyrano chromenes is reported. In this method, the synthesis of pyrano chromene derivatives was followed by using 4-hydroxycoumarin, malononit...

Journal: :Biomedical materials 2008
S A Manafi B Yazdani M R Rahimiopour S K Sadrnezhaad M H Amin M Razavi

In this study, hydroxyapatite (denoted as HAp) nanostructure with uniform morphologies, controllable size, nano-dispersion and narrow size distribution in diameter has been synthesized successfully by low-temperature hydrothermal process, and the as-synthesized powders were characterized by XRD, scanning electron microscopy, high-resolution transmission microscopy, FT-IR, Zetasizer and inductiv...

Journal: :Chemical communications 2011
Shan Xu Juyou Lu Hua Fu

A convenient and efficient copper-catalyzed cascade method has been developed for the synthesis of benzimidazoquinazoline derivatives via reactions of readily available substituted 2-(2-halophenyl)benzoimidazoles with amidines or guanidine under mild conditions (even at room temperature).

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