In the present work supercritical fluid extraction (SFE) using CO2, was applied for the pre-treatment of mandarin peels. Two-step extraction, combining SFE and conventional extraction, was investigated. During the first extraction step supercritical CO2 at temperatures 25, 40 and 60°C and pressures from 100 to 300 bar was applied to remove the non-polar components from the extracting material. ...

Several investigations on the extraction of dioxins from soil and fly ash with supercritical fluid have been reported; however, few of them describe the influence of components on the extraction. We extracted dioxins from eight samples with different values of organic carbon content and surface area with supercritical CO(2) at a temperature of 463 K, a pressure of 40 MPa, and using 10% toluene ...

There are two types of application for gas chromatography (GC) in the supercritical fluid extraction process. Gas chromatography is a type of supercritical extraction apparatuses which can separate a component from a multi-component mixture during supercritical extraction. Therefore, this application can be the alternative to conventional gas chromatography, which needs high temperatures for th...

This study examined the supercritical fluid extraction of wheat germ oil. The effects of pressure (200-300 bar at 40 degrees C) and extraction time on the oil quality/quantity were studied. A comparison was also made between the relative qualities of material obtained by SFE and by organic solvent extraction. The extracts were analyzed for alpha-tocopherol and polyunsaturated fatty acid content...

Let Ω be a bounded domain in Rn, n ≥ 3 with smooth boundary ∂Ω and a small hole. We give the first example of sign-changing bubbling solutions to the nonlinear elliptic problem −∆u = |u| n+2 n−2+ε−1u in Ω, u = 0 on ∂Ω, where ε is a small positive parameter. The basic cell in the construction is the signchanging nodal solution to the critical Yamabe problem −∆w = |w| 4 n−2w, w ∈ D(R) which has l...

A high-performance liquid chromatographic method is developed for use in the electrospray mass spectrometric (MS)-MS analysis of alkaloids contained in Cephalotaxus harringtonia leaves. Nine alkaloids having ester groups can be separated and detected with good sensitivity. The MS and MS-MS spectra obtained provides information on their chemical structures. Supercritical fluid extraction is also...

Supercritical Fluid Extraction have been used widely in the natural material industries ,because it produced excellent mass transfer properties, ease solubility control due to temperature and pressure. A mathematical model based on shrinking-core model of the extraction process and simulation were used. Previous worker’s have used a model including axial dispersion. They give the effect of an i...

Injecting liquid CO(2) into deep-sea sediments below ca. 3 km of seawater has been suggested for the permanent storage of anthropogenic CO(2). At the pressures and temperature found below 3 km of seawater, CO(2) becomes denser than seawater and so is likely to remain permanently sequestered in the sediment. Deepwater engineering, however, is expensive and seawater depths of greater than 3 km ar...

Vaccinium meridionale Swartz (Mortiño or Colombian blueberry) is one of the Vaccinium species abundantly found across the Colombian mountains, which are characterized by high contents of polyphenolic compounds (anthocyanins and flavonoids). The supercritical fluid extraction (SFE) of Vaccinium species has mainly focused on the study of V. myrtillus L. (blueberry). In this work, the SFE of Morti...