نتایج جستجو برای: situ crystallization
تعداد نتایج: 155287 فیلتر نتایج به سال:
Heating rate during crystallization is known to affect the final texture obtained in lead zirconate titanate thin films. The transient/intermediate phases present in the thin film during perovskite phase nucleation have been suggested to cause this variation in texture with heating rate. To understand the interrelationship between the transient/intermediate phases and the texture in the final p...
Nonlinear optical techniques are emerging as powerful in-situ probes of crystallization processes due to their inherent sensitivity crystal structure and morphology.
This paper presents a method to recognize polygonal-shaped particles (i.e. rectangles, regular/irregular prisms) among agglomerated crystals from in-situ images during a crystallization process. The aim is to measure the particle size distributions (PSD); a key measurement needed for monitoring and controlling industrial crystallization operations . The method is first based on detecting the ge...
Combining extensional rheology with in-situ synchrotron ultrafast x-ray scattering, we studied flow-induced phase behaviors of polyethylene (PE) in a wide temperature range up to 240 °C. Non-equilibrium phase diagrams of crystallization and melting under flow conditions are constructed in stress-temperature space, composing of melt, non-crystalline δ, hexagonal and orthorhombic phases. The non-...
The crystallization of calcium phosphate nanoparticles in the presence carboxylates was characterized situ through simultaneous SAXS/WAXS using synchrotron light.
The academic literature on and industrial practice of control of solution crystallization processes have seen major advances in the past 15 years that have been enabled by progress in in-situ real-time sensor technologies and driven primarily by needs in the pharmaceutical industry for improved and more consistent quality of drug crystals. These advances include the accurate measurement of solu...
Kinetic in situ neutron diffraction has been used to study the crystallization of amorphous Y67Fe33. The results show that partial crystallization first occurs close to 300 ◦C where the Y phase is formed. The entire sample crystallizes at 390 ◦C and new Bragg peaks appear, signifying the formation of a novel Y–Fe phase. This new phase coexists with Y to 450 ◦C when the Bragg peaks associated wi...
Precise protein structure determination provides significant information on life science research, although high-quality crystals are not easily obtained. We developed a system for producing high-quality protein crystals with high throughput. Using this system, gravity-controlled crystallization are made possible by a magnetic microgravity environment. In addition, in-situ and real-time observa...
نمودار تعداد نتایج جستجو در هر سال
با کلیک روی نمودار نتایج را به سال انتشار فیلتر کنید