نتایج جستجو برای: single crystal x
تعداد نتایج: 1554422 فیلتر نتایج به سال:
a two-dimensional nanolayered polyoxomolybdate, [4,4´-h2bipy] [mo7o22].h2o (1), where 4,4´-bipy = 4,4´-bipyridine, was prepared and characterized by ft-ir and atomic absorption spectroscopies, transmission electron microscopy (tem), x-ray single crystal and powder diffraction (xrd), and thermogravimetric analysis. the catalytic performance of 1 was assessed in the epoxidation of some olefins em...
the synthesis and single-crystal x-ray structure determination of the title compound [(bipy) , pb(0 ,cme) (o clo )] (1) and [(bipy) pb(clo ) ] (2) is described. compound (i) crystallizes in the triclinic space group p1(2), a= 7.384(2), b= 12.824(3), c= 10.622(6) a, ?= 73.41(2), ?= 80.98(2), ?= 73.68(2)', z= 2, and r =0.033 for 3408 independent reflections .compound (2) crystallizes in the ...
Copper(II) complex [Cu(dmbt)2(H2O)](ClO4)2 (1) was prepared from the reaction of copper(II) perchlorate hexahydrate with 2,2'-dimethyl-4,4'-bithiazole (dmbt) ligand in methanol at ambient temperature. The complex was quantitatively and qualitatively characterized by elemental analysis, absorption and infrared spectrometries. Complex [Cu(DMSO)5](ClO4)2 (2) was also synt...
Single crystals of Ba1-xKxBiO3 compound for 0 < x <0.6 from insulator to superconducting region have been grown by electrochemical method. The crystals have been characterized by powder x-ray diffraction and Laue x-ray to determine the crystal structure, formed phases and potassium concentration. Inelastic x-ray scattering spectrum of the crystals has been studied to investigate the phonon pro...
Template-free CuO nanorods were synthesized through a three-step chemical method with no water-insoluble materials. The first step included the preparation of a Cu-complex, which was obtained from dipicolinic acid, L-lysine, and copper nitrate. Then, as the second step, the obtained solution was allowed to be relaxed for a week to and formation of some blue single-crystals single crystals, whic...
Geometrical design of the spiral crystal selector can affect crystal orientation in the final single crystal structure. To achieve a better understanding of conditions associated with the onset of crystal orientation in a spiral crystal selector, temperature field was investigated using three-dimensional finite element method during the process. Different geometries of spiral crystal selec...
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