The MUNSON-WALKER method (3) with the modification of BERTRAND (1) has long been used for the determination of reducing sugars in plant extracts. The large amiiounts of solutions required by this method, however, make necessary the frequent preparation and standardization of solutions, which is inconvenient when large numbers of determinations are being made over an extended period of time. For...

A method is described for the estimation of adrenaline and noradrenaline in a 5 to 10 ml plasma sample.A batch technique of adsorption and elution from alumina is used and the final estimation is carried out using an automated fluorimetric technique based on the trihydroxyindole method. Fluorescence is stabilized first by thioglycollic acid to give noradrenaline concentrations only and then by ...

A new method is described for determining in shales the amount of sulphides that dissolve in dilute hydrochloric acid. 1he samples are treated with hydrochloric acid under vacuum, and the hydrogen sulphide evolved is absorbed in potassium hydroxide and titrated with potassium _~'~ermanganate. The analytical results are expressed as FeS. INTRODUCTION During a study of the distribution of the sul...

We consider the semiclassical limit of systems of autonomous PDE’s in 1+1 space-time dimensions in a scattering regime. We assume the matrix valued coefficients are analytic in the space variable and we further suppose that the corresponding dispersion relation admits real-valued modes only with one-dimensional polarization subspaces. Hence a BKW-type analysis of the solutions is possible. We t...

A comparison of methods, two based upon 5-hydroxymethylfurfural determination (colorimetric using a semi-automated procedure and HPLC) and ion exchange chromatography (HbA1 using BioRad method) was performed. The influence of variables on 5-hydroxymethylfurfural determination is reported. The dialysis step appears to be essential for an accurate determination of 5-hydroxymethylfurfural released...