8-33 (FeNH 4 (SO 4 ) 2 .12H 2 O) dissolved in 0.15 mL of 0.1 M HCl to 400 μg of CT dissolved in 1 mL of 68% aqueous methanol. (ii) Ascorbic acid concentrations in the final sample/reagent matrix of 0-400 μg mL -1 prepared in 1 mL of 68% aqueous methanol, containing 400 μg of CT. (iii) Sodium metabisulphite (Na 2 S 2 O 5 ) concentrations of 0-263 μg mL in the final sample/reagent matrix, prepare...

A spectrophotometric method has been developed for the determination of Cu(II) using Acetophenone 2’,5’dihydroxy, semicarbazone as an extractive reagent .The reagent forms a colored complex which has been quantitatively extracted into n-Butanol at pH 5.6. The method obeys Beer’s law over a range of 1 to 10 ppm. The molar absorptivity is 2564.1 L molcm and Sandell’s sensitivity is 0.02484 μg cm ...

Investigating the alkylation and acylation of N-acylthiazolidinethione, the desired α-alkylated products and C-acylated products are not obtained, but rather the S-alkylated products and O-acylated products are obtained. The possible mechanism proposed shows that the deprotonation agent and electrophilic species are responsible for the stability of enolates. The enolates derived from N-acylthia...