Distillation column is one of the most common operations in process industries and is while the most expensive unit of the amount of energy consumption. Many ideas have been presented in the related literature for optimizing energy consumption in distillation columns. This paper studies the different heat integration methods in a distillation column which separate Benzene, Toluene, Xylene, and ...

Distillation is not only the most energy consumer but also the most frequently-adopted separation operation in chemical industries since it separates a mixture only by the difference among vapor pressures (boiling points) of components. So distillation is often called as the king of separation processes. Therefore, research and development of technologies on energy savings of distillation is an...

INTRODUCTION In Japan, Pilot Plant of the HIDiC was built in 2005. It was commercial base scale and already achieved the consecutive distillation for 1000 hours. The energy consumption of the pilot HIDiC was only about 70% of that of a conventional distillation column. The HIDiC can lower reboiler and condenser load by heat exchange between rectifying section and stripping section. Therefore, i...

The esterification reaction between acetic acid and butanol was investigated in a reactive distillation column. The thermodynamic aspects of considered system are discussed, equilibrium constant, vapor pressures and UNIQUAC interaction parameters were investigated. Reactive distillation experiments were carried out to provide high purity butyl acetate. For this purpose, a 2 m column with nonrea...

The fully thermally coupled distillation column offers an alternative to conventional distillation towers, with the possibility of savings in both energy and capital costs. This innovative and promising alternative provides the opportunity to separate a multicomponent mixture into fractions with high purities merely in one column. A lack of knowledge still exists when dealing with the startup o...

The simulation and steady state operation of a vapor recompression pilot plant distillation column is studied in order to improve the thermal efficiency. A binary system of ethanol-water mixture is used. The simulation is carried through ASPEN PLUS version 9.3-1. Energy reduction of 89.26% is obtained comparing to the conventional distillation and the thermodynamic efficiency is improved from 1...

Multi-objective (energy–economic–safety) assessment of ethyl acetate production involving a heat pump is presented in this paper. The designed to intensify separation and reduce the total operating cost. Two pathways are upgraded using pump, conventional process reactive distillation column with unit. Detailed models including environment have been compiled optimized Aspen Plus software. Both b...

For the conceptual design of countercurrently operated reactive distillation columns, fast methods are needed to estimate potential top and bottom products. The possible column bottom product composition can be determined from the stable singular points of a batch reactive reboiler. In a similar manner the top product composition can be obtained from the stable singular points of a batch reacti...

In this work, we obtain and compare the control properties of thermally coupled reactive distillation sequences and thermally coupled extractive distillation sequences with those of conventional reactive and extractive distillation configurations. All sequences have been designed using a multiobjective genetic algorithm with restrictions. The theoretical control properties of those schemes were...