This study reports an analytical method for the determination of nitroimidazole and quinolones in honey using liquid chromatography-tandem mass spectrometry (LC-MS/MS). A modified QuEChERS methodology was used to extract the analytes and determine veterinary drugs in honey by LC-MS/MS. The linear regression was excellent at the concentration levels of 1-100 ng/mL in the solution standard curve ...

A fast and simple modified QuEChERS (quick, easy, cheap, rugged and safe) extraction method based on spiked calibration curves and direct sample introduction was developed for determination of Benzo [a] pyrene (BaP) in bread by gas chromatography-mass spectrometry single quadrupole selected ion monitoring (GC/MS-SQ-SIM). Sample preparation includes: extraction of BaP into acetone followed by cl...

Three different calibration approaches were applied in HPLC/MS/MS using electrospray ionization for the determination of 14 diverse pesticide residues at different levels in a variety of food matrixes. This study was conducted as part of a 4 day training course for 17 chemists to learn the "quick, easy, cheap, effective, rugged, and safe" (QuEChERS) approach to pesticide residue analysis in foo...

The determination of zearalenone (ZEN) and its derivatives as biomarkers in animal tissues or organs plays an important role in mycotoxin monitoring and can promote effective exposure assessment. A liquid chromatography-tandem mass spectrometry (LC-MS/MS) method for the simultaneous quantification of nine ZEN-like mycotoxins, including three glucuronides in different pig tissues (heart, liver, ...

QuEChERS stands for (Quick, Easy, Cheap, Effective, Rugged and Safe) and pronounced as (catchers) is a method that had been developed for multi-pesticide residue analyses in food. This study was conducted to investigate the efficacy of QuEChERS method for analyzing the organochlorine pesticides residues in cow's milk. Twenty organochlorine pesticide namely (Benzene, 1,3,5-trichloro, Tetrachloro...

Since the middle of last century, the use of organic synthetic pesticides became a widespread practice, in order to better prevent, control and destroy pests. Despite their usefulness in the increment of food production, the extensive use of pesticides during production, processing, storage, transport or marketing of agricultural commodities can led to environmental contamination and to the pre...

Varietal thiols are important contributors to the aroma profile of a wide range beverages including beer. A methodology for simultaneous extraction and subsequent analysis varietal 3-sulfanylhexan-1-ol (3SH), 3-sulfanylhexylacetate (3SHA) 4-methyl-4-sulfanylpentan-2-one (4MSP), non-volatile precursors 3-S-cysteinylhexan-1-ol (Cys-3SH) 3-S-glutathionylhexan-1-ol (GSH-3SH) in beer was developed v...

A method for the determination of pesticide residues in water and sediment was developed using the QuEChERS method followed by gas chromatography--mass spectrometry. The method was validated in terms of accuracy, specificity, linearity, detection and quantification limits. The recovery percentages obtained for the pesticides in water at different concentrations ranged from 63 to 116%, with rela...