نتایج جستجو برای: preparation of cis 3 azido 4 styryl 2 azetidinone

تعداد نتایج: 21671370  

Journal: :Acta Crystallographica Section E Structure Reports Online 2008

Journal: :Acta Crystallographica Section E Structure Reports Online 2010

2017
Jan Pícha Miloš Buděšínský Kateřina Macháčková Michaela Collinsová Jiří Jiráček

The rise of CuI-catalyzed click chemistry has initiated an increased demand for azido and alkyne derivatives of amino acid as precursors for the synthesis of clicked peptides. However, the use of azido and alkyne amino acids in peptide chemistry is complicated by their high cost. For this reason, we investigated the possibility of the in-house preparation of a set of five Fmoc azido amino acids...

Journal: :Acta Crystallographica Section E Structure Reports Online 2008

Journal: :Organic letters 2015
Fei Yu Matthew S McConnell Hien M Nguyen

The highly α-selective and scalable synthesis of the Fmoc-protected GalNAc-threonine amino acid and TN antigen in gram scale (0.5-1 g) is described. The challenging 1,2-cis-2-amino glycosidic bond is addressed through a coupling of threonine residues with C(2)-N-ortho-(trifluoromethyl)benzylidenamino trihaloacetimidate donors mediated by Ni(4-F-PhCN)4(OTf)2. The desired 1,2-cis-2-amino glycosid...

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