Powder activated carbon surface (AC) was grinded and modified and altered procedure thorough a facile and easy chemical reaction to appearance of 2-((3silylpropylimino)1-methyl) phenol (AC- (SPIMP)). Subsequently, this novel sorbent efficiently applied for the extraction and preconcentration of some metal ions from real samples. Preliminary the influences of variables such as pH, amounts of rea...

In this study, Santa Barbara Amorphous (SBA-15) mesoporous silica has been functionalized with aminopropyl groups that were converted to propargyl-bearing moieties through the reaction with propargyl bromide. The material then underwent an efficient Cu(I)-catalyzed azide alkyne click reaction with sodium azide in order to obtain the corresponding triazole products. The covalent modification of ...

The analysis of an 11-hour series of high resolution white light observations of a large pore in the sunspot group NOAA 7519, observed on 5 June 1993 with the Swedish Vacuum Solar Telescope at La Palma on Canary Islands, has been recently described by Dorotovič et al. (2002). Special attention was paid to the evolution of a filamentary region attached to the pore, to horizontal motions around t...

In this study, Santa Barbara Amorphous (SBA-15) mesoporous silica has been functionalized with aminopropyl groups that were converted to propargyl-bearing moieties through the reaction with propargyl bromide. The material then underwent an efficient Cu(I)-catalyzed azide alkyne click reaction with sodium azide in order to obtain the corresponding triazole products. The covalent modification of ...

A two-step acid/base-catalyzed silica gel has been aged in alcohol and water baths followed by various aprotic solvents with a wide range of surface tensions. Low temperature (CO 2) and high temperature (ethanol) aerogels were also prepared. The physical and chemical structures of gels dried from aprotic solvents were studied by a series of techniques (29Si MAS-NMR, nitrogen adsorption, SAXS, e...

in this paper, the development of a new potassium carbonateon alumina support sorbent prepared byimpregnating k2co3 with an industrial grade of al2o3 support was investigated. the co2 capturecapacity was measured using real flue gas with 8% co2 and 12% h2o in a fixed-bed reactor at atemperature of 65 °c using breakthrough curves. the developed sorbent showed an adsorptioncapacity of 66.2 mgco2/...

In this research effect of synthesis method of magnesium aluminate as support of Ni catalysts at the reverse water gas shift (RWGS) reaction was evaluated. The RWGS reaction is applied in Carbon Dioxide Hydrogenation to Form Methanol via a Reverse Water-Gas Shift Reaction (CAMERE) process for the transformation of CO2 into methanol. The MgAl2O4 supports were prepared by sol-gel (M1), surfactant...

mesoporous  mgo  microstructures  were  synthesized  using magnesium  acetate  tetrahydrate,  ammonium  oxalate  monohydrate and  pluronic  f127  via  heating  at  40  °c  for  24  h  and  subsequent calcination. the mesoporous structure of magnesium oxide with the specific  surface  area  of  47m2/g,  pore  volume  0.30  cm3/g  and  the average pore size 24 nm is produced. according to xrd stu...

in this work, bsea-sba-15 was prepared for the first time, which was prepared by covalently anchoring schiff-base compound (n,n´-bis(salicylidene)ethylenediamine (bsea) on sba-15 by hydrothermal method. the structure and physicochemical properties were determined by elemental analysis, xrd, nitrogen adsorption–desorption, thermogravimetric analysis and ftir spectroscopy, sem, bet surface area a...