The electroreduction of the pertechnetate ions has been examined in sulfuric acid solutions (0.5-4 M) using optically transparent thin layer spectroelectrochemical (RVC-OTTLE) cell. Soluble Tc(III), TcO2+ and [Tc(μ-O)2Tc]3+/4+ species with absorption bands at 420-450, 400, and 502 nm, respectively, were found to be formed during the reduction of TcO4- ions. The strongly acidic medium was found ...

INTRODUCTION Variceal haemorrhage is a potentially life-threatening complication in cirrhotic patients. Identification of patients at high risk for bleeding is particularly important. The aim of this study was to determine the clinical usefulness of per-rectal portal scintigraphy (PPS) in the evaluation of the severity of portal hypertension in cirrhotic patients, in terms of correlation betwee...

To determine the factors associated with 20 minute Tc-99m pertechnetate thyroid uptake, we examined all patients in whom thyrotoxicosis was diagnosed at Chiba-Hokusoh Hospital, Nippon Medical School from 2001 April through 2003 March. Patients with thyrotoxicosis diagnosed during this period were 57 with Graves' disease (76%), 11 with transient hyperthyroxinemia (TH)(14.7%), and 7 with subacute...

OBJECTIVE To investigate in vivo and in humans the mechanisms and kinetics of vagina-to-uterus distribution. DESIGN Controlled clinical study. SETTING Volunteers in an academic research environment. PATIENT(S) Six postmenopausal women undergoing transabdominal hysterectomy were selected. INTERVENTION(S) Women received 0.2 mL of (99m)Tc-pertechnetate vaginally. In three patients the cerv...

To the Editor: The development and introduction of the UltraTag® kit (Mallinckrodt, Inc., St. Louis, MO) offered a substantial improvement in the ability to conveniently and efficiently radiolabel red blood cells with mTc (1 ). This particular cell-labeling technique is especially desirable for use in studies of gastrointestinal hemorrhage (GI bleed) since even minimal levels of free pertechnet...

OBJECTIVE The purpose of this study was to investigate if an octadecyl (18C) minicolumn could be applied successfully for quality control of 99mTc exametazime (HMPAO). METHODS The 18C column system using saline eluent was validated against the Whatman 17 method in calculating the percent radiochemical purity of 99mTc-HMPAO. The behavior of 99mTc-pertechnetate (99mTc04-) and hydrolyzed-reduced...

Follicular thyroid carcinoma is common in regions with insufficient iodine diets and represents approximately 10-20 % of all thyroid malignancies1,2. The treatment of patients suffering from follicular thyroid carcinoma includes surgery and radioiodine therapy3. Although after definitive therapy, the survival of these patients is good, these patients need to be followed for local recurrences an...

Leonidas, J. C., and Germann, D. R. (1974). Archives of Disease in Childhood, 49, 21. Technetium-99m pertechnetate imaging in diagnosis of Meckel's diverticulum. Abdominal imaging after intravenous injection of 99mTc pertechnetate is a simple, safe, and noninvasive diagnostic procedure to show ectopic gastric mucosa, which is present in most cases of symptomatic Meckel's diverticulum. It was pe...

Technetium-99m aprotinin was prepared from an optimised radiolabelling kit formulation containing aprotinin, alkaline buffer and stannous chloride (reducing agent) and radiolabelled using (99m) Tc-pertechnetate. The labelling was achieved within 25 min, with radiochemical purities of >98%.