in this paper, nickel oxide (nio) nanoparticles have been prepared by solid state thermal decomposition of an acyclic nickel(ii) complex (1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(ii) chloride, [nil]cl2, in an electrical furnace at optimal temperature, 450 ºc for 3.5 h. the nickel(ii) complex is obtained via solid state synthesis using nickel(ii) chloride and tetradentate o4 acyclic ligan...

The growing process of a spinel-like oxide film can be obtained through different atmospheres; in this sense Air, O2, steam, and nitrogen atmospheres were used steps during the aging heat treatment at 490ºC maraging 300 350 alloys. oxidation layer produced under was chemically, microstructurally mechanically characterized by means advanced techniques. results showed (in both alloys) non-homogen...

A detailed study of the methanol chemisorption and oxidation processes on oxide surfaces allowed the development of a method to quantify the number of surface active sites (Ns) of metal oxide catalysts. In situ infrared analysis during methanol adsorption showed that molecular methanol and surface methoxy species are co-adsorbed on an oxide surface at room temperature, but only surface methoxy ...

Abstract A series of supported Ni-Mo catalysts were synthesised through a deposition-co-precipitation method (DcP) and investigated in combined steam dry reforming. The prepared by Yttria-Stabilised Zirconia (YSZ), Gadolinium-Doped Ceria (GDC) Stabilised (CSZ) with improved carbon tolerance have the potential to be used as anodes Solid Oxide Fuel Cells (SOFC). These will applied anode supportin...

This paper reports the performance of nickel oxide based electrode in alkaline anion exchange membrane water electrolysis. The membrane used is polystyrene based alkaline membrane and the electrode used is Nickel as cathode and Nickel oxide as anode. The electrochemical activity of the Nickel oxide is high compared to uncoated electrode. The AWE membrane electrode gave high current density at 3...

Oxide Dispersion Strengthened (ODS) and TZM molybdenum have excellent creep resistance and strength at high temperatures in inert atmospheres. Fracture toughness and tensile testing was performed at temperatures between -1 50°C and 450°C to characterize 6.35 mm thick plate material of ODS and TZM molybdenum. A transition from low fracture toughness values (5.8 to 29.6 MPaJm) to values > 30 MPaJ...

in this study, a mixed matrix polyethersulfone/iron-nickel oxide nanoparticle nanofiltration membrane was prepared by the solution casting technique. polyvinylpyrrolidone was also used as a membrane pore former in membrane fabrication. the effect of iron-nickel oxide nanoparticles concentration in the casting solution on the membrane structure and performance was investigated. scanning optical ...

molybdenum thin films with 50 and 150 nm thicknesses were deposited on silicon substrates, using dc magnetron sputtering system, then post-annealed at different temperatures (200, 325, 450, 575 and 700°c) with flow oxygen at 200 sccm (standard cubic centimeter per minute). the crystallographic structure of the films was obtained by means of x-ray diffraction (xrd) analysis. an atomic force micr...

The ferrochrome alloy is produced by electric arc melting of the mineral chromite (FeCr2O4). It is largely used for the production of stainless steels. Increasing the amount of chromium content in the steel allows for increased corrosion and oxidation resistance. Other alloying elements, such as nickel (Ni) or molybdenum (Mo), aid in making the steel more passive and increasing its stainless pr...