Mixed cryoprotectants have been developed for the solubilization of ligands for crystallization of protein-ligand complexes and for crystal soaking. Low affinity lead compounds with poor solubility are problematic for structural studies. Complete ligand solubilization is required for co-crystallization and crystal soaking experiments to obtain interpretable electron density maps for the ligand....

introduction: to examine the long-term effects of normal saline and a synthetic tissue fluid (phosphate buffered saline, pbs) on mineral trioxide aggregate (mta). materials and methods: root-ends of twelve extracted human teeth were resected; root-end cavities were prepared and filled with mta. samples were randomly divided into two groups of six each. teeth in group i were placed in normal sal...

-The chemical composition of mixed-layer serpentine/chlorite (Sp/Ch) in Tuscaloosa Formation sandstone was analyzed by energy dispersive X-ray spectroscopy (EDX) in the scanning electron miscroscope (SEM) and by X-ray diffraction (XRD). EDX results indicate little depth-controlled variation in composition, whereas XRD results suggest distinct decreases in octahedral Fe and tetrahedral A1. XRDde...

The alpha-aminoisobutyric (Aib) residue has generally been considered to be a strongly helicogenic residue as evidenced by its ability to promote helical folding in synthetic and natural sequences. Crystal structures of several peptide natural products, peptaibols, have revealed predominantly helical conformations, despite the presence of multiple helix-breaking Pro or Hyp residues. Survey of s...

We fabricate mixed halide perovskite films through dual-source vacuum deposition of PbX2 (X = Cl, Br, and I) and methyl ammonium iodide (MAI) precursors with various deposition ratios. Vacuum deposition is an optimal way for film fabrication because it gives a uniform perovskite film which is free from contamination such as metallic phase lead, residual solvent, and moisture. The ionization pot...

In the present study, the ice slurry refrigeration system with pre-cooling heat exchanger (ISSH) is studied experimentally to achieve the system performance, ice crystal formation time and the temperature of ice crystal formation. The operating parameters considered in this paper include the concentration of salt solution, suction pressure, discharge pressure and Energy Efficiency Ratio (EER). ...

The Eocene-Oligocene Sarbisheh volcanic complex is a part of the Lut-Sistan Zone that outcrops in eastern Iran. In the east of this complex, three groups of volcanic rocks (i.e., andesite, dacite, and rhyolite) exist. Plagioclase as the main mineral of these rocks is found with varying micro-textures. Based on a changing trend in the concentration of anorthite, the developed micro-textures (coa...

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