نتایج جستجو برای: microwave hydrothermal

تعداد نتایج: 67304  

2009
SA Eliziário LS Cavalcante JC Sczancoski PS Pizani JA Varela JWM Espinosa E Longo

In this letter, we report on the obtention of hafnium oxide (HfO(2)) nanostructures by the microwave-hydrothermal method. These nanostructures were analyzed by X-ray diffraction (XRD), field-emission gum scanning electron microscopy (FEG-SEM), transmission electron microscopy (TEM), energy dispersive X-ray spectrometry (EDXS), ultraviolet-visible (UV-vis) spectroscopy, and photoluminescence (PL...

2017
Boris I. Kharisov Oxana V. Kharissova Ubaldo Ortiz Méndez

2011
Swapan Kumar Sarkar Byong Taek Lee

Bioactive glasses were synthesized in an inexpensive hydrothermal chemical route by the use of microwave energy irradiation. Compositional changes were carried out to synthesis bioactive glass with different Si content. Densification behavior was investigated by microwave sintering process from 700 °C to 1000 °C temperature. The powders were characterized for their physical and morphological ch...

2016
Lian-Hua Fu Yan-Jun Liu Ming-Guo Ma Xue-Ming Zhang Zhi-Min Xue Jie-Fang Zhu

In this paper, we report a facile, rapid, and green strategy for the synthesis of cellulose/hydroxyapatite (HA) nanocomposites using an inorganic phosphorus source (sodium dihydrogen phosphate dihydrate (NaH2PO4·2H2O)), or organic phosphorus sources (adenosine 5′-triphosphate disodium salt (ATP), creatine phosphate disodium salt tetrahydrate (CP), or D-fructose 1,6-bisphosphate trisodium salt o...

Reducing the consumption of cement with simultaneous utilizing waste materials as cement replacement is preferred for reasons of environmental protection. Blended cements consist of different supplementary cementitious materials (SCMs), such as fly ash, silica fume, Ground Granulated Blast Furnace Slag (GGBFS), natural pozzolans, etc. These materials should be chemically activated to show effec...

Journal: :Physical chemistry chemical physics : PCCP 2010
Jishu Han Hao Zhang Haizhu Sun Ding Zhou Bai Yang

In the conventional procedure of the preparation of aqueous semiconductor nanocrystals (NCs), the growth of NCs was mainly through the thermodynamics-favored Ostwald ripening process. It required additional energy to promote NC growth, such as reflux, hydrothermal method, microwave irradiation, and sonochemical synthesis. Energy-promoted growth usually led to the decomposition of mercapto-ligan...

Journal: :Journal of colloid and interface science 2012
Yongliang Li Jiajun Wang Yong Zhang Mohammad Norouzi Banis Jian Liu Dongsheng Geng Ruying Li Xueliang Sun

Birnessite flower-like and α-type tubular MnO(2) nanostructures were selectively synthesized through simple decomposition of KMnO(4) under hydrochloric acid condition by controlling reaction temperature using a microwave-assisted hydrothermal method. The as-prepared samples were characterized in detail by various techniques including X-ray diffraction, field emission scanning electron microscop...

Journal: :Nanoscale 2013
Ji-Young Kim Kwang-Heon Kim Seung-Beom Yoon Hyun-Kyung Kim Sang-Hoon Park Kwang-Bum Kim

An in situ chemical synthesis approach has been developed to prepare ruthenium oxide/reduced graphene oxide (RGO) nanocomposites. It is found that as the C/O ratio increases, the number density of RuO2 nanoparticles decreases, because the chemical interaction between the Ru ions and the oxygen-containing functional groups provides anchoring sites where the nucleation of particles takes place. F...

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