background & aim:nepeta racemosa is an herbal and medicinal plant and this report aims to   identify chemical compositions of the essential oils and volatiles of its   aerial parts through classical and advanced methods.  experimental: chemical profiles of the essential oils and volatile compounds from the aerial parts of nepeta racemosa obtained through hydrodistillation (hd), solvent-free mic...

Several applications such as liquid-liquid extraction in micro-fluidic devices are concerned with the flow of two immiscible liquid phases. The commonly observed flow regimes in these systems are slug-flow and stratified flow. The latter regime in micro-channels has the inherent advantage that separation of the two liquids at the exit is efficient. Recently extraction in a stratified counter-cu...

The direct coupling of in-tube solid-phase microextraction (in-tube SPME) with microcolumn liquid chromatography (micro-LC) has been investigated for the analysis of antidepressants in human urine. The use of in-tube SPME has been clearly shown to be advantageous for the on-line coupling of the SPME method, as the sample pretreatment technique, with micro-LC as the separation technique. This is...

This article reviews the recent developments in Bio-Analytical sample preparation techniques and gives an update on basic principles, Applications and comparative discussion on the advantages and limitations of each technique. Conventional Solid-Phase Extraction (SPE), Molecularly Imprinted Polymer SPE techniques are have been considered as methods of past. Developments in SPE techniques such a...

We have developed and evaluated a rapid, high-pressure liquid-chromatographic method for theophylline in serum. Only 0.2 ml of serum is required for each determination, and the sensitivity of this method is 0.5 mg/liter. This method, involving liquid extraction and silica adsorption chromatography, provides adequate selectivity, accuracy, and precision for routine or research applications. Litt...

artificial neural networks (anns) are computer techniques that attempt to simulate the functionality and decision-making processes of the human brain. in the past few decades, artificial neural networks (anns) have been extensively used in a wide range of engineering applications. there are only a few applications in liquid membrane process. the objective of this research was to develop artific...

We describe an analysis for propranolol in plasma, with use of reversed-phase "high-pressure" liquid chromatography and fluorescence detection. Pronethalol is used as the internal standard. The procedure, which involves extraction into an organic solvent, evaporation, and clean-up by micro-scale back extraction from hexane into an aqueous phase, is specific and sensitive. The detection limit is...

In the conventional multiphase flow, immiscible having a liquid-liquid interface, two liquids are merged in flow path to form interface. The two-phase separation mixed solution has property of phase-separating from one phase phases by changing temperature/pressure, and phase-separates into upper lower batch-type vessel. By while sending this micro-space region, interface is formed obtained. Thi...

The present study was carried out between September 2019 and March 2020 in Yıldız River, which is located within the borders of Yıldızeli district Sivas province used for agricultural irrigation purposes, to determine chemical characteristics river water trace elements. Water’s alkalinity, oxygen demand (COD), chloride (Cl-), calcium (Ca2+), total hardness, phosphate (PO4-P), dissolved reactive...