نتایج جستجو برای: high pressure liquid
تعداد نتایج: 2491478 فیلتر نتایج به سال:
RP-HPLC of analogues of oxytocin containing a reduced peptide bond was studied using various columns and buffers. Anomalous behavior of one analogue served as a basis for the discussion of possible conformational consequences of this substitution.
The pharmacokinetics of colistin was investigated using specific high-performance liquid chromatography (HPLC) to measure the concentrations of colistin and colistin A and B in plasma and urine in five rats after administration of an intravenous bolus of 1 mg of colistin sulfate/kg of body weight. There were differences in the pharmacokinetic behaviors of unbound colistin A and B. This is the f...
Solid-state extraction of plasma or serum offers significant advantages over traditional liquid-liquid methods in cortisol determinations by liquid chromatography (HPLC). Sample preparation is facilitated and HPLC column contamination is minimized. Extract yield from the solid-state columns is enhanced by sample pretreatment with methanol. Cortisol values by solid-state extraction/HPLC correlat...
Hexazinone has been detected at levels ranging from 0.2 to 50 micrograms/L in many groundwater samples from eastern Maine over the past decade. A rapid and inexpensive direct-injection high-performance liquid chromatographic (HPLC) method has been developed to monitor contamination levels of the herbicide. The method is sensitive (limit of quantitation = 0.33 microgram/L) and is linear to 33.0 ...
front matter & 2009 a.2010.01.002 author. : diegochiappetta@y Abstract Objective: Two carvedilol aqueous solutions and one carvedilol aqueous suspension for paediatric oral use (1mg/ml) were studied to determine their stability. Method: All samples were stored at 4, 25 and 401C. Carvedilol content of each of the three formulations was tested using high performance liquid chromatography (HPLC). ...
A review of indirect photometric and fluorometric detection in high-performance liquid chromatography (HPLC) is presented. A functional definition of indirect detection, somewhat broader and simpler than what was often used to characterize these techniques, was employed for this review. Emphasis was placed on distinguishing different approaches to indirect photometric and fluorometric detection...
When analyses of mixtures of small molecules are carried out at mobile phase velocities close to (for isocratic runs) or somewhat above (for gradient runs) the optimum velocity, the eddy diffusion term contributes to at least 75% of the band broadening. Future improvements in column performance may come only from a reduction of the eddy diffusion term. The classical models of axial dispersion o...
Determination of 1-nitropyrene in low volume ambient air samples by HPLC with fluorescence detection
*KURAに登録されているコンテンツの利用については,著作権法に規定されている私的使用や引用などの範囲内で行ってください。 *著作権法に規定されている私的使用や引用などの範囲を超える利用を行う場合には,著作権者の許諾を得てください。ただし,著作権者 から著作権等管理事業者(学術著作権協会,日本著作出版権管理システムなど)に権利委託されているコンテンツの利用手続については ,各著作権等管理事業者に確認してください。 Title Determination of 1-nitropyrene in low volume ambient air samples by high-performance liquid chromatography with fluorescence detection Author(s) Ohno, Takanori; Toriba, Akira; Kameda...
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The 1,6- and 1,7-regioisomers of dinitro- (1,6-A and 1,7-A) and diamino-substituted perylene bisimides (1,6-B and 1,7-B), and 1-amino-6-nitro- and 1-amino-7-nitroperylene bisimides (1,6-C and 1,7-C) were synthesized. The 1,6-A and 1,7-A regioisomers were successfully separated by high performance liquid chromatography and characterized by 500 MHz 1H-NMR spectroscopy, and subsequently, their red...
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