water soluble chitosan oligosaccharide (cho) was hydrophobically modified with camptothecin (cpt) in different molar ratios of cpt, and characterized by ft-ir and 1 h-nmr spectroscopy. nanomicelles prepared by these copolymers were analyzed for size, zeta, and length of time they remain stable. the critical micelle concentration (cmc) and dissociation of micelles at physiological ph and acidic ...

NMR spectroscopy is the go-to technique for determining the solution structures of organic, organometallic, and even macromolecular species. However, structure determination of nanoscale aqueous inorganic clusters by NMR spectroscopy remains an unexplored territory. The few hydroxobridged inorganic species well characterized by H Nuclear Magnetic Resonance spectroscopy (H-NMR) do not provide en...

From the aerial parts of Tanacetum balsamita L. (Compositae) a flavonol aglycon was iso­lated using chromatographic techniques. The structure of this compound was determined using spectroscopic methods (UV, H-NMR and MS) as 3',4',5,7-Tetrahydroxy flavonol (Quercetin).

2H Magic-angle spinning nuclear magnetic resonance (MAS NMR), echo 27Al NMR, two-dimensional (2D) echo 1H MAS NMR and 1H, 27Al and 29Si MAS NMR have been applied to study the acid sites of dehydrated zeolites. The quadrupole coupling constants CQCC determined from 2H MAS NMR spectra of Si-OH-Al sites increase with the framework aluminium content of the zeolites from 208 Hz (H-ZSM-5) to 236 kHz ...

From the aerial parts of Tanacetum balsamita L. (Compositae) a flavonol aglycon was iso­lated using chromatographic techniques. The structure of this compound was determined using spectroscopic methods (UV, H-NMR and MS) as 3',4',5,7-Tetrahydroxy flavonol (Quercetin).

H(2)O@C(60) derivatives covalently linked to a nitroxide radical were synthesized. The (1)H NMR of the guest H(2)O revealed the formation of many isomers with broad signals. Reduction to the diamagnetic hydroxylamines sharpened the (1)H NMR signals considerably and allowed for an "isomer count" based on the number of observed distinct signals. For H(2)O@K-8, 17 positional isomeric nitroxides ar...