In this work a rapid and selective procedure for separation and preconcentration of lead(Pb2+) before determination by electrothermal atomic absorption spectrometry (ETAAS) wasdeveloped. The procedure is based on the electrodeposition on a graphite probe modified withpalladium. The lead was deposited from acetate buffer solution at pH 5.5. Various parameters,such as pH of solutions, deposition ...

lichen species (hypogymnia physodes and evernia prunastri) were used for biomonitoring thepossible air pollution with heavy metals in the vicinity of copper mine in the eastern part of the republic ofmacedonia. the contents of 18 elements were analysed by icp-aes and etaas techniques. for dataprocessing basic statistical methods and multivariate exploratory (factor and cluster analysis) techniq...

in this work a rapid and selective procedure for separation and preconcentration of lead(pb2+) before determination by electrothermal atomic absorption spectrometry (etaas) wasdeveloped. the procedure is based on the electrodeposition on a graphite probe modified withpalladium. the lead was deposited from acetate buffer solution at ph 5.5. various parameters,such as ph of solutions, deposition ...

lichen species (hypogymnia physodes and evernia prunastri) were used for biomonitoring thepossible air pollution with heavy metals in the vicinity of copper mine in the eastern part of the republic ofmacedonia. the contents of 18 elements were analysed by icp-aes and etaas techniques. for dataprocessing basic statistical methods and multivariate exploratory (factor and cluster analysis) techniq...

A simple microextraction method based on solidification of a floating organic drop (SFOD) was developed for preconcentration of lead prior to its determination by electrothermal atomic absorption spectrometry (ETAAS). Ammonium pyrolidinedithiocarbamate (APDC) was used as complexing agent, and the formed complex was extracted into a 20 μL of 1-undecanol. The extracted complex was diluted with et...