نتایج جستجو برای: dta tga

تعداد نتایج: 8405  

Journal: :physical chemistry research 0
ensieh ghasemian lemraski ilam university soheila sharafinia ilam university masoud alimohammadi ilam university

this paper presents a systematic study of the surface chemistry, porous texture and adsorptive characteristics of prepared new activated carbon using persian mesquite grain. several techniques and methodologies such as, proximate analysis, n2 adsorption–desorption isotherms, scanning electron microscope (sem), fourier transform infrared spectroscopy(ft-ir), x-ray diffraction (xrd), x-ray photoe...

Journal: :Jurnal Teori dan Aplikasi Fisika 2023

The aim of this research is to make wollastonite from silica obtained rice husk ash and commercial calcium carbonate using the solids reaction method. DTA-TGA results show mass due evaporation H2O decomposition CaCO3 into CaO along with calcination temperature, in addition, DTA also identify formation β-CaSiO3 phase α-CaSiO3 phase. XRD were dominated by minor was indicated peak intensity which ...

2011
Mamdouh M. Abou-Mesalam

A novel hydrothermal zirconium oxide (ZrO2) ion exchange material was successfully synthesized by hydrothermal technique. The material has been characterized using different tools such as thermal analysis (DTA-TGA), FT-IR and X-ray diffraction studies. The results show that the prepared ZrO2 is pure and with a unique shape and it belongs to the hexagonal system. Chemical resistively of the mate...

Journal: :AIP Advances 2022

LiNi 1?x-0.02 Mg 0.02 Co x O 2 compounds with = 0.0, 0.02, 0.04, 0.06, and 0.08 compositions are prepared by the solid-state method. Their thermal, structural, morphological, functional, first cycle charge/discharge studies were carried out help of thermogravimetric analysis (TGA)/differential thermal (DTA), XRD, SEM, FTIR, a biologic galvanostat respectively. The TGA/DTA shows their structural...

Journal: :Sains Malaysiana 2021

Polyvinyl benzyl chloride (PVBC) was synthesized by free radical polymerization of 4-vinylbenzyl using benzoyl peroxide initiator at 60 °C. PVBC synthesised in different solvents such as toluene, xylene, 1,4-dioxane, and tetrahydrofuran. The polymers were structurally characterized 1H NMR FTIR spectroscopic techniques. thermal property the polymer investigated thermogravimetric analysis (TGA) d...

Journal: Journal of Nanoanalysis 2018
Maryam Gorjizadeh Mina Javdannezhad Mohammad Hosein Sayahi, Soheil Sayyahi,

Caffeine loaded magnetic nanoparticle was successfully synthesized and were characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray analysis (EDX), thermo gravimetric analysis (TGA), differential thermal analysis (DTA) and vibrating sample magnetometer (VSM). The resulting nanocom...

Ali Morsali, Azadeh Askarinejad Mohammad Amin Alavi

Nanocrystalline ZnO particles were prepared by a novel sonochemical route from zinc acetate and sodium hydroxide without any requirement of calcination steps at high temperature and without surfactants. Variations in several parameters and their effects on the structural (crystal size and morphology) properties of nanoparticles were investigated. Characterizations were carried out by X-Ray ...

M. Bahmanyar M. Masteri-Farahani, M. Mohammadikish

Silica  coated magnetite  nanoparticles were  covalent  grafted with  3-aminopropyl trimethoxysilane  to give APTSCMNPs. Reaction of  the resulted nanomaterial with 4-formyl benzo-12-crown-4 ether afforded FB12C4/APTSMNPs  nanocomposite  material  in  which  the  crown ether  moiety  was  attached  through  propyl  chain  spacer. Characterization of  the prepared nanocomposite was performed wit...

Journal: :journal of physical & theoretical chemistry 2007
m. rafizadeh

a new metal-organic compound, [fe(pydc)(dmso)(h2o)cl], (where pydc is pyridine-2, 6-dicarboxylate and dmso is dimethyl sulfoxide), has been synthesized and characterized by singlecrystal x-ray diffraction, tga/dta, ir and raman spectroscopy. green-yellow crystals,crystallized in the monoclinic system, space group p21/n, a = 7.2461(4) å, b = 10.3018(4) å, c =17.7667(10) å, α = 90°, β = 90.014°(5...

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